SIMULTANEOUS CAPILLARY GC-MS DETERMINATION OF TRIAZINES AND AMIDES IN WATER

文献类型: 外文期刊

第一作者: Berthion, JM

作者: Berthion, JM;Bodereau, I;Fournier, J

作者机构:

关键词: Gas chromatography mass spectrometry;Triazines;Amides;Water pollution;Solid-phase extraction

期刊名称:CHROMATOGRAPHIA ( 影响因子:2.044; 五年影响因子:1.725 )

ISSN:

年卷期:

页码:

收录情况: SCI

摘要: A simultaneous capillary Gas Chromatographic-Mass Spectrometric (GC-MS) method is described for the determination of thirteen pesticides belonging to the triazine and amide families in water. The sample is extracted in liquid-liquid mode (dichloromethane) and then the determination of the residues is carried out by capillary gas chromatography with mass spectrometric detection in the Selected-Ion Monitoring mode (SIM). The average recoveries of spiked compounds are in the 78.4-135.4 % range between the relative low level (0.100 mu g L(-1)) and the relative high level (10.0 mu g L(-1)). The limits of detection (LOD) are in the 0.009-0.128 mu g L(-1) range. [References: 14]

分类号: O65

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