文献类型： 外文期刊
第一作者： Wang, Dan
作者： Wang, Dan;Wan, Zhaohua;Zhang, Heng;Yi, Hong;Lei, Aiwen;Wang, Dan;Alhumade, Hesham;Alhumade, Hesham;Lei, Aiwen
作者机构：
关键词： diarylamine; electrochemistry; homogeneous catalysis; metal-free; reductive arylation
期刊名称：CHEMSUSCHEM （ 影响因子：8.928； 五年影响因子：8.868 ）
ISSN： 1864-5631
年卷期：
页码：
收录情况： SCI
摘要： The synthesis of diarylamine is extremely important in organic chemistry. Herein, a novel electrochemical reductive arylation of nitroarenes with arylboronic acids was developed. A variety of diarylamines were synthesized without the need for transition-metal catalysts. The reaction could be scaled up efficiently in a flow cell and several derivatization reactions were carried out smoothly. Cyclic voltammetry experiments and mechanism studies showed that acetonitrile, formic acid, and triethyl phosphite all played a role in promoting this reductive arylation transformation.
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