Optimizing Ultrasound-Assisted Deep Eutectic Solvent Extraction of Bioactive Compounds from Chinese Wild Rice

文献类型： 外文期刊

第一作者： Zeng, Jia

作者： Zeng, Jia;Dou, Yuqing;Yan, Ning;Li, Na;Zhang, Huaibao;Tan, Jia-Neng;Zeng, Jia;Li, Na;Tan, Jia-Neng

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关键词： deep eutectic solvents; Chinese wild rice; bioactive compounds; response surface methodology; UPLC-QqQ-MS

期刊名称：MOLECULES （ 影响因子：4.411； 五年影响因子：4.587 ）

ISSN：

年卷期： 2019 年 24 卷 15 期

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收录情况： SCI

摘要： In this study, deep eutectic solvents (DESs) were used for the ultrasound-assisted extraction (UAE) of valuable bioactive compounds from Chinese wild rice (Zizania spp.). To this end, 7 different choline chloride (CC)-based DESs were tested as green extraction solvents. Choline chloride/1,4-butanediol (DES-2) exhibited the best extraction efficiency in terms of parameters such as the total flavonoid content (TFC), total phenolic content (TPC), and free radical scavenging capacity (DPPH. and ABTS(.+)). Subsequently, the UAE procedure using 76.6% DES-2 was also optimized: An extraction temperature of 51.2 degrees C and a solid-liquid ratio of 37.0 mg/mL were considered optimal by a Box-Behnken experiment. The optimized extraction procedure proved efficient for the extraction of 9 phenolic and 3 flavonoid compounds from Chinese wild rice as determined by quantification based on ultra-performance liquid chromatography-triple quadrupole tandem mass spectrometry (UPLC-QqQ-MS). This work, thus, demonstrates the possibility of customizing green solvents that offer greater extraction capacity than that of organic solvents.

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