Simultaneous Determination of Five Benzimidazoles in Feeds Using High-Performance Capillary Electrophoresis

文献类型： 外文期刊

第一作者： Shen, Jianzhong

作者： Shen, Jianzhong;Tong, Jing;Jiang, Haiyang;Li, Na;Guo, Liming;Ding, Shuangyang;Rao, Qinxiong

作者机构：

关键词： animal feed;poultry feed;swine feed

期刊名称：JOURNAL OF AOAC INTERNATIONAL （ 影响因子：1.913； 五年影响因子：1.754 ）

ISSN：

年卷期：

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收录情况： SCI

摘要： A high-performance capillary electrophoretic method for determination of five benzimidazoles (thiabendazole, albendazole, fenbendazole, mebendazole, oxfendazole) in animal feeds was developed. Separation was carried out in an 80.5 cm x 75 mu m id fused-silica uncoated capillary and injected by hydrodynamic injection (35 mbar x 8 s) at a wavelength detection of 295 nm. The drugs were completely resolved in 50 mmol/L citric acid buffer (pH 1.9) with 30 W at a temperature of 25 degrees C. Linear range was 1-80 mu g/mL; limits of detection for the analytes were less than 2 mg/kg; the overall recoveries for benzimidazoles were >73%, with coefficients of variation below 10%.

分类号： O65

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