Residue Depletion of Imidocarb in Swine Tissue

文献类型： 外文期刊

第一作者： Wang, Zhongjie

作者： Wang, Zhongjie;Wang, Yongjian;Wu, Wenxue;Li, Xiubo;Li, Yijing;Wu, Lianyong

作者机构：

关键词： Imidocarb;swine;residue depletion;intramuscular administration;HPLC-UV

期刊名称：JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY （ 影响因子：5.279； 五年影响因子：5.269 ）

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年卷期：

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收录情况： SCI

摘要： A residue depletion study was performed with high-performance liquid chromatography(HPLC)to determine a withdrawal period of imidocarb(IMD)in swine tissues.The drug was administered intramuscularly(im)at the dose of 2.0 mg kg~(-1)of body weight(bw)once a day for 3 days.Samples of muscle,fat,liver,kidney,and injection site muscle from 5 pigs were collected on 7,14,28,and 56 days after the last administration.Quantitative analysis of IMD was conducted by HPLC-UV at 260 nm after liquid-liquid extraction.The limit of detection(LOD)of the method was 0.1 mu g g~(-1)for liver and kidney and 0.05 mu g g~(-1)for muscle and fat,respectively.Mean recoveries of IMD in all fortified samples at a concentration range of 0.1-25,mu g g~(-1)were 69.5-89.3%,with a coefficient of variation(CV)below 13.3%.In swine,the highest drug levels occurred in liver and kidney during the whole study period,suggesting that these tissues are targets for residues.IMD concentrations in all examined tissues were below the accepted maximum residue limits(MRLs)recommended by the Committee for Veterinary Medical Products(CVMP)of the European Medical Evaluation Agency(EMEA)at 54 days post-treatment.

分类号： S13

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