Determination of cyflumetofen residue in water, soil, and fruits by modified quick, easy, cheap, effective, rugged, and safe method coupled to gas chromatography/tandem mass spectrometry

文献类型： 外文期刊

第一作者： Liu, Xingang

作者： Liu, Xingang;Dong, Fengshou;Xu, Jun;Zheng, Yongquan;Li, Minmin;Zheng, Yongquan;Qin, Dongmei

作者机构：

关键词： Cyflumetofen acaricides;Fruits;Residue analysis

期刊名称：JOURNAL OF SEPARATION SCIENCE （ 影响因子：3.645； 五年影响因子：2.943 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A new, highly sensitive, and selective method was developed for the determination of the cyflumetofen residue in water, soil, and fruits by using gas chromatography quadruple mass spectrometry. The target compound was extracted using acetonitrile and then cleaned up using dispersive solid-phase extraction with primary and secondary amine and graphitized carbon black, and optionally by a freezing-out cleanup step. The matrix-matched standards gave satisfactory recoveries and relative standard deviation values in different matrices at three fortified levels(0.05, 0.5, and 1.0 mg kg -1). The overall average recoveries for this method in water, soil, and all fruits matrix at three fortified levels ranged from 76.3 to 101.5% with relative standard deviations in the range of 1.2-11.8%(n = 5). The calculated limits of detection and quantification were typically below 0.005 and 0.015 μg kg ~(-1), which were much lower than the maximum residue levels established by Japanese Positive List. This study provides a theoretical basis for China to draw up maximum residue level and analytical method for cyflumetofen acaricide in different fruits.

分类号： O6

  • 相关文献

[1]Residue analysis of four diacylhydrazine insecticides in fruits and vegetables by Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method using ultra-performance liquid chromatography coupled to tandem mass spectrometry. Liu, Xingang,Xu, Jun,Dong, Fengshou,Li, Yuanbo,Zheng, Yongquan,Song, Wenchen.

[2]Rapid residue analysis of four triazolopyrimidine herbicides in soil, water, and wheat by ultra-performance liquid chromatography coupled to tandem mass spectrometry. Liu, Xingang,Xu, Jun,Li, Yuanbo,Dong, Fengshou,Li, Jing,Zheng, Yongquan,Song, Wenchen.

[3]Multiresidue determination of benzoylurea insecticides in vegetable matrices. He Hongmei,Wu Liqin,Zhang Hu,Zhu Jiahong,Xie Lei. 2006

[4]Residue analysis and risk assessment of tebuconazole in jujube (Ziziphus jujuba Mill). You, Xiangwei,Li, Yiqiang,Wang, Xiuguo,Xu, Jinli,Zheng, Xiao,Sui, Chengcheng.

[5]Multiplug filtration cleanup method with multi-walled carbon nanotubes for the analysis of malachite green, diethylstilbestrol residues, and their metabolites in aquatic products by liquid chromatography-tandem mass spectrometry. Qin, Yuhong,Zhang, Jingru,Li, Yanjie,Han, Yongtao,Zou, Nan,Pan, Canping,Jiang, Yanbin,Shan, Jihao.

[6]Application of SPME Based on a stainless steel wire for the determination of pyrethroid insecticide residues in water and soil. Jia, Chunhong,Zhu, Xiaodan,Zhao, Ercheng,Yu, Pingzhong,He, Min,Chen, Li.

[7]Residue Determination of cis-Epoxiconazole Enantiomers in Fruit and Tea by Ultra Performance Convergence Chromatography Combined with Quadrupole Time-of-Flight Mass Spectrometry. Zhao Yue-Chen,Cui Xin-Yi,Zhang Xin-Zhong,Luo Feng-Jian,Zhou Li,Chen Zong-Mao. 2016

[8]Validated hydrophilic interaction LC-MS/MS method for determination of 2-pyrrolidinone residue: Applied to a depletion study of 2-pyrrolidinone in swine liver. Liu, Yanhong,Chen, Ximing,Ji, Yanhong,Chen, Jiangtao,Wang, Guangxiang,Shang, Youjun,Liu, Xiangtao,Pan, Jack.

[9]Distribution and elimination of Norfloxacin in Fenneropenaeus chinensis larvae. Sun Ming,Sun Ming,Li Jian,Zhao Fazhen,Li Jitao,Chang Zhiqiang. 2013

[10]Extraction of organophosphorus pesticides in water and juice using ultrasound-assisted emulsification-mixroextraction. Jia, Chunhong,Zhu, Xiaodan,Chen, Li,He, Min,Yu, Pingzhong,Zhao, Ercheng.

[11]Extraction of pesticides in water samples using vortex-assisted liquid-liquid microextraction. Jia, Chunhong,Zhu, Xiaodan,Zhao, Ercheng,He, Min,Chen, Li,Yu, Pingzhong,Jia, Chunhong,Zhu, Xiaodan,Wang, Jihua,Zhao, Ercheng,He, Min,Chen, Li,Yu, Pingzhong.

[12]Determination of 16 insect growth regulators in edible Chinese traditional herbs by liquid chromatography electrospray tandem mass spectrometry. Qian, Mingrong,Wu, Liqin,Zhang, Hu,Xu, Mingfei,Li, Rui,Wang, Xiangyun,Sun, Caixia.

[13]Residue Analysis of Forchlorfenuron in Fruit and vegetable by RP-HPLC. Zhang, Hua,Yang, Xin,Dong, Ai Jun,Ma, Ying,Wang, Zhen Yu,Yang, Lin,Zhang, Ying Chun,Yang, Xin,Wang, Jing. 2010

[14]Antioxidant activity of polyphenol and anthocyanin extracts from fruits of Kadsura coccinea (Lem.) AC Smith. Yao, Jinyan,Huang, Shaoxi,Sun, Jian,Wang, Jubing,Garcia-Garcia, Elena,Garcia-Garcia, Elena. 2009

[15]Principles, developments and applications of computer vision for external quality inspection of fruits and vegetables: A review. Zhang, Baohua,Huang, Wenqian,Li, Jiangbo,Zhao, Chunjiang,Fan, Shuxiang,Wu, Jitao,Zhang, Baohua,Zhao, Chunjiang,Liu, Chengliang. 2014

[16]Determination of imidacloprid,carbendazim and thiabendazole residues in vegetables and fruits by HPLC. Lin, Ling,Peng, Zheng,Yang, Chunliang,Wang, Mingyue,Zha, Yubing,Liu, Lili,Zeng, Shaodong. 2013

[17]Simultaneous Determination of Five Plant Growth Regulators in Fruits by Modified Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) Extraction and Liquid Chromatography-Tandem Mass Spectrometry. Shi, Xiaomei,Jin, Fen,Huang, Yuting,Du, Xinwei,Wang, Miao,Shao, Hua,Jin, Maojun,Wang, Jing,Li, Chunmei.

[18]Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction. Chen, Fang,Chen, Lanzhen,Zhou, Jinhui,Xue, Xiaofeng,Zhao, Jing,Wang, Qiang.

[19]Cumulative risk assessment of the exposure to pyrethroids through fruits consumption in China - Based on a 3-year investigation. Li, Zhixia,Nie, Jiyun,Xu, Guofeng,Yan, Zhen,Li, Zhixia,Nie, Jiyun,Xu, Guofeng,Yan, Zhen,Lu, Zeqi,Xie, Hanzhong,Kang, Lu,Chen, Qiusheng,Li, An,Zhao, Xubo.

[20]Monitoring, exposure and risk assessment of sulfur dioxide residues in fresh or dried fruits and vegetables in China. Lou, Tiantian,Huang, Weisu,Wu, Xiaodan,Wang, Mengmeng,Lu, Baiyi,Hu, Yinzhou,Huang, Weisu,Zhou, Liying,Zheng, Lufei.

作者其他论文 更多>>

微信小程序