Ionic liquid-based ultrasonic/microwave-assisted extraction combined with UPLC-MS-MS for the determination of tannins in Galla chinensis

文献类型： 外文期刊

第一作者： Lu, Chunxia

作者： Lu, Chunxia;Wang, Hongxin;Lv, Wenping;Ma, Chaoyang;Lou, Zaixiang;Xie, Jun;Liu, Bo

作者机构：

关键词： Galla chinensis;ionic liquid;tannins;ultrasonic/microwave-assisted extraction;UPLC-MS/MS

期刊名称：NATURAL PRODUCT RESEARCH （ 影响因子：2.861； 五年影响因子：2.572 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： Ionic liquid was used as extraction solvents and applied to the extraction of tannins from Galla chinensis in the simultaneous ultrasonic- and microwave-assisted extraction (UMAE) technique. Several parameters of UMAE were optimised, and the results were compared with of the conventional extraction techniques. Under optimal conditions, the content of tannins was 630.2±12.1mgg 1. Compared with the conventional heat-reflux extraction, maceration extraction, regular ultrasound- and microwave-assisted extraction, the proposed approach exhibited higher efficiency (11.7-22.0% enhanced) and shorter extraction time (from 6h to 1min). The tannins were then identified by ultraperformance liquid chromatography tandem mass spectrometry. This study suggests that ionic liquid-based UMAE is an efficient, rapid, simple and green sample preparation technique.

分类号： R9

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