Determination of Herbicide Propisochlor in Soil, Water and Rice by Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Method Using by UPLC-ESI-MS/MS

文献类型： 外文期刊

第一作者： Xu, Jun

作者： Xu, Jun;Liu, Xingang;Dong, Fengshou;Zheng, Yongquan;Wu, Yanbing;Zhang, Ying

作者机构：

关键词： Propisochlor;UPLC-MS/MS;Rice;Soil;Water

期刊名称：BULLETIN OF THE KOREAN CHEMICAL SOCIETY （ 影响因子：0.969； 五年影响因子：0.691 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A simple, quick and reliable analytical method for the confirmation and quantification of propisochlor was developed. The propisochlor was extracted from water, soil and rice (stalks, rice and hull) matrices using acetonitrile, and cleaned up with primary secondary amine and determined by UPLC-MS/MS. The LODs of propisochlor ranged from 0.03 ug/kg to 0.12 ug/kg, while the LOQs ranged from 0.1 ug/kg to 0.4 ug/kg in different matrixes. The mean recoveries of propisochlor at three levels (0.005, 0.01 and 0.05 mg/kg) were in the range of 73.7-94.9% with intra-day relative standard deviations (RSD) of 1.1-13.9% and inter-day RSD_R of 3.3-12.7%. This method is suitable for routine analysis of propisochlor under field conditions. The half-lives of propisochlor in rice stalks, water and soil were 1.7, 1.5 and 2.3 days in Hunan, 5.7, 1.0 and 1.9 days in Anhui and 4.8, 1.0 and 3.1 days in Guangxi.

分类号： O6

  • 相关文献

[1]Enantioseparation and Determination of the Chiral Fungicide Furametpyr Enantiomers in Rice, Soil, and Water by High-Performance Liquid Chromatography. Chen, Xiu,Xu, Jun,Liu, Xingang,Chen, Zenglong,Li, Yuanbo,Zheng, Yongquan,Zhang, Hongjun.

[2]Influence of a heavy rainfall event on the leaching of [C-14]isoproturon and its degradation products in outdoor lysimeters. Doerfler, Ulrike,Cao, Guoyin,Grundmann, Sabine,Schroll, Reiner.

[3]Multi-element pollution in soil, ground and surface water from abandoned chromate chemical plants: a case study in Hangzhou, China. Zou, Lina,Wang, Shaoxian,Hashmi, Muhammad Z.,Tang, Xianjin,Shi, Jiyan,Wang, Shaoxian,Liu, Lei,Liu, Lei. 2015

[4]Rapid residue analysis of four triazolopyrimidine herbicides in soil, water, and wheat by ultra-performance liquid chromatography coupled to tandem mass spectrometry. Liu, Xingang,Xu, Jun,Li, Yuanbo,Dong, Fengshou,Li, Jing,Zheng, Yongquan,Song, Wenchen.

[5]Enantioselective separation of the carfentrazone-ethyl enantiomers in soil, water and wheat by HPLC. Dong, Fengshou,Liu, Xingang,Xu, Jun,Chen, Wuying,Cheng, Li,Ning, Ping,Li, Jing,Zheng, Yongquan,Wang, Yunhao.

[6]Transmission Efficiency of Cucumber green mottle mosaic virus via Seeds, Soil, Pruning and Irrigation Water. Li, Jun-Xiang,Liu, Shan-Shan,Gu, Qin-Sheng.

[7]Rapid residue analysis of oxathiapiprolin and its metabolites in typical Chinese soil, water, and sediments by a modified quick, easy, cheap, effective, rugged, and safe method with ultra high performance liquid chromatography and tandem mass spectrometry. Ju, Chao,Dong, Fengshou,Liu, Xingang,Wu, Xiaohu,Zhao, Huanhuan,Zheng, Yongquan,Xu, Jun.

[8]Petroleum contamination of soil and water, and their effects on vegetables by statistically analyzing entire data set. Zhang, Juan,Du, Xiao-ming,Li, Fa-sheng,Hou, Hong,Yang, Jun-cheng,Fan, Shu-kai.

[9]Development of a multi-residue enantiomeric analysis method for 9 pesticides in soil and water by chiral liquid chromatography/tandem mass spectrometry. Dong, Fengshou,Liu, Xingang,Xu, Jun,Chen, Xiu,Han, Yongtao,Liang, Xuyang,Zheng, Yongquan.

[10]Atmospheric pressure gas chromatography quadrupole-time-of-flight mass spectrometry for simultaneous determination of fifteen organochlorine pesticides in soil and water. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wu, Xiaohu,Chen, Zenglong,Pan, Xinglu,Zheng, Yongquan.

[11]Simultaneous measurements of cations and anions using diffusive gradients in thin films with a ZrO-Chelex mixed binding layer. Wang, Yan,Ding, Shiming,Shi, Lei,Gong, Mengdan,Xu, Shiwei,Zhang, Chaosheng.

[12]Dissipation of chlorpyrifos and residue analysis in rice, soil and water under paddy field conditions. Zhang, Xiao,Shen, Yan,Yu, Xiang-yang,Liu, Xian-jin,Zhang, Xiao.

[13]Determination of chlorantraniliprole residues in corn and soil by UPLC-ESI-MS/MS and its application to a pharmacokinetic study. Xu, Jun,Liu, Xingang,Li, Jing,Li, Yuanbo,Kong, Zhiqiang,Zheng, Yongquan,Shan, Weili,Zheng, Zuntao.

[14]Heavy Metal Contamination in a Soil-Rice Ecosystem in the Vicinity of Abandoned Rural Unsanitary Landfill. Guan, Yidong,Guan, Yidong,Du, Yehong,Zhang, Zhiyuan,Ge, Chuan,Luo, Ancheng,La, Gui-xiao,Cao, Jie.

[15]Temporal changes of radiocesium in irrigated paddy fields and its accumulation in rice plants in Fukushima. Yang, Baolu,Ha, Yiming,Yang, Baolu,Onda, Yuichi,Wakiyama, Yoshifumi,Yoshimura, Kazuya,Sekimoto, Hitoshi.

[16]Soil organic sulfur mineralization in the presence of growing plants under aerobic or waterlogged conditions. Li, ST,Lin, B,Zhou, W. 2001

[17]Diazotrophic diversity, nifH gene expression and nitrogenase activity in a rice paddy field in Fujian, China. Martensson, Lotta,Diez, Beatriz,Wartiainen, Ingvild,El-Shehawy, Rehab,Rasmussen, Ulla,Zheng, Weiwen.

[18]Earthworms enhanced winter oilseed rape (Brassica napus L.) growth and nitrogen uptake. Zhang, Shujie,Chao, Ying,Zhang, Chunlei,Cheng, Jing,Li, Jun,Ma, Ni.

[19]N, P Contribution and soil adaptability of four arbuscular mycorrhizal fungi. Wenke, Liu.

[20]Protective function of narrow grass hedges on soil and water loss on sloping croplands in Northern China. Xiao, Bo,Wang, Qing-hai,Wu, Ju-ying,Huang, Chuan-wei,Yu, Ding-fang,Xiao, Bo.

作者其他论文 更多>>

微信小程序