Determination of Gossypol in Poultry Egg and Feed by Automated Solid-Phase Extraction and High-Performance Liquid Chromatography

文献类型: 外文期刊

第一作者: Shi, Zu-Hao

作者: Shi, Zu-Hao;Tang, Meng-Jun;Zhang, Xiao-Yan;Tao, Zhi-Yun;Wu, Ming;Gao, Yu-Shi;Gu, Rong;Lu, Jun-Xian;Pu, Jun-hua;Ge, Qing-Lian

作者机构:

关键词: Gossypol;High-performance liquid chromatography;Egg;Poultry feed.

期刊名称:ASIAN JOURNAL OF CHEMISTRY ( 影响因子:0.355; 五年影响因子:0.293 )

ISSN:

年卷期:

页码:

收录情况: SCI

摘要: A high-performance liquid chromatographic method for the determination of gossypol in poultry egg and feed was developed. Gossypol was extracted with 90 % acetonitrile/water (v/v) in presence of ascorbic acid and purified by C_(18)cartridge with automated solid-phase extraction system. The samples were separated through an optimized chromatography condition on a C_(18) column (4.6 mm x 250 mm, 5 μm particle) and UV detection at 235 nm. A gradient with acetonitrile and water containing 0.1 % phosphoric acid was applied. The method was shown to be highly reproducible, with overall recovery was 89.5 % and relative standard deviation was 8.7 %.

分类号: O6

  • 相关文献

[1]Niemann-Pick C2 Proteins: A New Function for an Old Family. Guo, Mengbuo,Liu, Yang,Pelosi, Paolo,Wang, Guirong,Ban, Liping,Song, Li-Mei. 2018

[2]Temporal allocation of metabolic tolerance in the body of beet armyworm in response to three gossypol-cotton cultivars. Wu Gang,Guo JianYing,Wan FangHao,Wu Gang,Harris, Marvin K.. 2009

[3]Effects of different sources and levels of dietary gossypol on gossypol residues in plasma and milk of lactating cows. Wang, A. P.,Zhang, J. M.,Meng, Y. L.,Deng, L. Q.,Lv, Y. F.,Li, C.,Wang, J. Q.,Wang, A. P.,Lv, Y. F.. 2012

[4]Metabolic Characterization of Dairy Cows Treated with Gossypol by Blood Biochemistry and Body Fluid Untargeted Metabolome Analyses. Tang, Chaohua,Zhang, Kai,Zhan, Tengfei,Zhao, Qingyu,Zhang, Junmin,Tang, Chaohua,Zhang, Kai,Zhan, Tengfei,Zhao, Qingyu,Zhang, Junmin.

[5]Design, Synthesis, and Biological Activities of Aromatic Gossypol Schiff Base Derivatives. Li, Ling,Li, Zheng,Wang, Kailiang,Liu, Yuxiu,Wang, Lizhong,Li, Yongqiang,Wang, Qingmin,Li, Jiarui,Yang, Peiwen,Shang, Hui,Zhao, Sheng,Feng, Jiming.

[6]Metabolic engineering of gossypol in cotton. Zhou, Meiliang,Zhang, Chengcheng,Wu, Yanmin,Tang, Yixiong. 2013

[7]Mapping quantitative trait loci for cottonseed oil, protein and gossypol content in a Gossypium hirsutum x Gossypium barbadense backcross inbred line population. Yu, Jiwen,Yu, Shuxun,Fan, Shuli,Song, Meizhen,Zhai, Honghong,Li, Xingli,Zhang, Jinfa.

[8]Multi-omics analyses of red blood cell reveal antioxidation mechanisms associated with hemolytic toxicity of gossypol. Tang, Chaohua,Meng, Qingshi,Zhang, Kai,Zhan, Tengfei,Zhao, Qingyu,Zhang, Junmin,Tang, Chaohua,Meng, Qingshi,Zhang, Kai,Zhan, Tengfei,Zhao, Qingyu,Zhang, Junmin,Zhang, Sheng. 2017

[9]Effect of dietary fatty acids on serum parameters, fatty acid compositions, and liver histology in Shaoxing laying ducks. Liu, Wei-meng,Lu, Li-zhi,Zhang, Jing,Tao, Zheng-rong,Shen, Jun-da,Li, Guo-qin,Wang, De-qian,Li, Jin-jun,Tian, Yong,Liu, Wei-meng,Lai, Shu-jing,Shi, Fang-xiong,Zhang, Jing,Liu, Yu,Yu, Bo. 2011

[10]Determination of Mycotoxin Biomarkers in Eggs by Liquid Chromatography-Tandem Mass Spectrometry Coupled with Matrix Solid Phase Dispersion. Zhu Run-Yue,Xu Fei,Zhu Run-Yue,Zhao Zhi-Yong,Song Su-Quan,Yang Xian-Li,Nie Dong-Xia,Wu Ai-Bo,Song Su-Quan. 2015

[11]Analysis of Ribavirin and Its Metabolites in Fresh Eggs by Ultra High Performance Liquid Chromatography-Tandem Mass Spectrometry. Qi Kai,Tang Xiao-Yan,Wang Min,Zheng Xin,Yang Meng-Rui,Zhou Jian,Qi Kai,Zheng Xin. 2016

[12]Effects of an aqueous alfalfa extract on production performance, egg quality and lipid metabolism of laying hens. Deng, W.,Dong, X. F.,Tong, J. M.,Xie, T. H.,Zhang, Q.. 2012

[13]A simple sample pretreatment method for multi-mycotoxin determination in eggs by liquid chromatography tandem mass spectrometry. Zhu, Runyue,Zhao, Zhiyong,Yan, Liping,Song, Suquan,Zhao, Zhiyong,Wang, jianhua,Bai, Bing,Wu, Aibo,Song, Suquan,Wu, Aibo,Zhu, Runyue.

[14]Bithionol residue analysis in animal-derived food products by an effective and rugged extraction method coupled with liquid chromatography-tandem mass spectrometry. Zheng, Weijia,Park, Jin-A,Abd El-Aty, A. M.,Kim, Seong-Kwan,Cho, Sang-Hyun,Choi, Jeong-Min,Yi, Hee,Cho, Soo-Min,Kim, Jin-Suk,Shin, Ho-Chul,Abd El-Aty, A. M.,El-Banna, H. A.,Shim, Jae-Han,Chang, Byung-Joon,Wang, Jing.

[15]Embryotropic actions of follistatin: paracrine and autocrine mediators of oocyte competence and embryo developmental progression. Rajput, Sandeep K.,Lee, KyungBon,Guo Zhenhua,Folger, Joseph K.,Smith, George W.,Guo Zhenhua,Di, Liu. 2014

[16]Determination of Polybrominated Diphenyl Ethers and Derivatives, Tetrabromobisphenol A, Hexabromocyclododecane in Egg Samples by Gel Permeation Chromatography and Dispersive Solid Phase Extraction. Li Min-Jie,Jin Fen,Yang Li-Li,Wu Ri-Na,Shao Hua,Jin Mao-Jun,Wang Jing. 2014

[17]Egg Safety Standards in China Need To Be Improved. Zhang, Guoyou,Chen, Ailiang,Zhao, Yan,Xu, Zhenzhen,Chen, Gang,Yang, Shuming,Zhang, Guoyou,Chen, Ailiang,Zhao, Yan,Xu, Zhenzhen,Chen, Gang,Yang, Shuming.

[18]Simultaneous determination of six synthetic phenolic antioxidants in edible oils using dispersive liquid-liquid microextraction followed by high-performance liquid chromatography with diode array detection. Shuangjiao Xu,Liangliang Liu,Yanqin Wang,Dayun Zhou,Meng Kuang,Dan Fang,Weihua Yang,Shoujun Wei,Aiping Xiao,Lei Ma.

[19]A simple and economic method for simultaneous determination of 11 antibiotics in manure by solid-phase extraction and high-performance liquid chromatography. Feng, Yao,Zhang, Wenjuan,Liu, Yuanwang,Li, Zhaojun,Hu, Haiyan,Wei, Chaojun,Zhang, Wenjuan,Xue, Jianming. 2016

[20]Using beta-cyclodextrin/attapulgite-immobilized ionic liquid as sorbent in dispersive solid-phase microextraction to detect the benzoylurea insecticide contents of honey and tea beverages. Yang, Miyi,Wu, Xiaoling,Xi, Xuefei,Zhang, Panjie,Yang, Xiaoling,Lu, Runhua,Zhou, Wenfeng,Zhang, Sanbing,Gao, Haixiang,Li, Jianyong.

作者其他论文 更多>>