Analysis of (-)-shikimic acid in Chinese star anise by GC-MS with selected ion monitoring

文献类型： 外文期刊

第一作者： Liu, Hongcheng

作者： Liu, Hongcheng;Li, Qiwan;Zhou, Yanhong;Liu, Hongcheng;Zhang, Yin

作者机构：

关键词： (-)-Shikimic acid;Chinese star anise (Illicium verum Hook. f.);Gas chromatography-mass spectrometry;Selected ion monitoring

期刊名称：CHROMATOGRAPHIA （ 影响因子：2.044； 五年影响因子：1.725 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A sensitive, specific, accurate, and reproducible GC-MS method with selected ion monitoring for quantitative determination of (-)-shikimic acid (SA) in Chinese star anise, using benzoic acid as internal standard, has been developed and validated. The homogeneity of the sample was evaluated by one way analysis of variance. The extraction efficiency of ultrasound-assisted and Soxhlet extraction was compared. Results showed that ultrasonic extraction was as efficient as Soxhlet extraction but was more rapid and simpler. Linearity and recovery were good. The method was used for analysis of (-)-SA in Chinese star anise from different areas in Wenshan state, Yunnan province. It was found that Chinese star anise collected from Pingbian and Funing counties contained more (-)-SA than other samples, with two plants from Pingbian county containing >15% (-)-SA.

分类号： O65

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