A multiplex approach for the UPLC-PDA-MS/MS data: analysis of licorice

文献类型: 外文期刊

第一作者: Pan, Lang-Sheng

作者: Pan, Lang-Sheng;Liu, Ping-Le;Goncalves, Carlos Miguel Vicente;Dong, Nai-Ping;Liang, Yi-Zeng;Lv, Hui-Ying;Li, Ya-Ping

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期刊名称:ANALYTICAL METHODS ( 影响因子:2.896; 五年影响因子:2.716 )

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收录情况: SCI

摘要: Ultra-performance liquid chromatography (UPLC) coupled to photodiode array detection (PDA) and electrospray ionization (ESI) tandem mass spectrometry (MS) methods was developed to separate and characterize the chemical components in licorice. Pure ultraviolet (UV) spectra were extracted using chemometric methods, and pure mass spectra were obtained using rankmap analysis. After the acquirement of the pure mass spectra, the isotopic structure peaks of molecular ions were optimized using Origin software, which could provide some help for the qualitative analysis. Pure mass spectra could also provide the correct parent ion for further tandem MS analysis. Finally, sixty compounds were identified.

分类号: O65

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