Simple and sensitive monitoring of beta(2)-agonist residues in meat by liquid chromatography-tandem mass spectrometry using a QuEChERS with preconcentration as the sample treatment

文献类型： 外文期刊

第一作者： Xiong, Lin

作者： Xiong, Lin

作者机构：

关键词： QuEChERS;beta(2)-Agonists;LC-MS/MS;Feed additive;Meat;DVB-NVP-SO3Na

期刊名称：MEAT SCIENCE （ 影响因子：5.209； 五年影响因子：5.305 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A liquid chromatography with tandem mass spectrometric detection (LC-MS/MS) method was established for the simultaneous determination of the levels of 10 beta(2)-agonists in meat. The samples were extracted using an aqueous acidic solution and cleaned up using a Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) technique utilising a DVB-NVP-SO3Na sorbent synthesised in-house. First, the beta(2)-agonist residues were extracted in an aqueous acidic solution, followed by matrix solid-phase dispersion for clean-up. The linearities of the method were R-2 = 0.9925-0.9998, with RSDs of 2.7-15.3% and 73.7-103.5% recoveries. Very low limits of detection (LOD) and quantitation (LOQ) of 02-0.9 mu g/kg and 0.8-3.2 mu g/kg, respectively, were achieved for spiked meat. The values obtained were lower than the maximum residue limits (MRLs) established by the EU and China. These results clearly demonstrate the feasibility of the proposed approach. The evaluated method provided reliable screening, quantification and identification of 10 beta(2)-agonists in meat. (C) 2015 Elsevier Ltd. All rights reserved.

分类号： TS25

  • 相关文献

[1]A method for multiple identification of four beta(2)-Agonists in goat muscle and beef muscle meats using LC-MS/MS based on deproteinization by adjusting pH and SPE for sample cleanup. Xiong, Lin,Gao, Ya-Qin,Li, Wei-Hong,Guo, Tian-Feng,Yang, Xiao-Lin,Xiong, Lin,Gao, Ya-Qin,Li, Wei-Hong,Guo, Tian-Feng,Yang, Xiao-Lin. 2015

[2]Rapid Determination of Chlormequat in Meat by Dispersive Solid-Phase Extraction and Hydrophilic Interaction Liquid Chromatography (HILIC)-Electrospray Tandem Mass Spectrometry. Li, Chunmei,Jin, Fen,Qi, Yamei,Shi, Xiaomei,Wang, Miao,Shao, Hua,Jin, Maojun,Wang, Jing,Li, Chunmei,Yang, Mingqi,Yu, Zhiyong.

[3]A simple sample pretreatment method for multi-mycotoxin determination in eggs by liquid chromatography tandem mass spectrometry. Zhu, Runyue,Zhao, Zhiyong,Yan, Liping,Song, Suquan,Zhao, Zhiyong,Wang, jianhua,Bai, Bing,Wu, Aibo,Song, Suquan,Wu, Aibo,Zhu, Runyue.

[4]Simultaneous determination of five pyrazole fungicides in cereals, vegetables and fruits using liquid chromatography/tandem mass spectrometry. Chen, Xiu,Liu, Xingang,Xu, Jun,Li, Yuanbo,Zheng, Yongquan,Shan, Weili.

[5]Determination of Fluazinam in Vegetables and Fruits Using a Modified QuEChERS Method and Liquid Chromatography-Tandem Mass Spectrometry. Li, Yubo,Tang, Hongxia,Dong, Maofeng,Wang, Weimin,Song, Weiguo,Black, Kezia C..

[6]Determination of hymexazol in 26 foods of plant origin by modified QuEChERS method and liquid chromatography tandem-mass spectrometry. Jiang, Zejun,Li, Hui,Cao, Xiaolin,Du, Pengfei,Shao, Hua,Jin, Fen,Jin, Maojun,Wang, Jing.

[7]Simultaneous determination of carbamate insecticides and mycotoxins in cereals by reversed phase liquid chromatography tandem mass spectrometry using a quick, easy, cheap, effective, rugged and safe extraction procedure. Zhang, Jin-Ming,Lu, Yao-Bin,Wu, Yin-Liang.

[8]Development and validation of a simple and fast method for simultaneous determination of aflatoxin B-1 and sterigmatocystin in grains. Zhao, Yarong,Ma, Liyan,Zhao, Yarong,Huang, Jianxiang,Wang, Fuhua,Zhao, Yarong,Huang, Jianxiang,Wang, Fuhua,Zhao, Yarong,Huang, Jianxiang,Wang, Fuhua.

[9]Determination and Dissipation of Fipronil and Its Metabolites in Peanut and Soil. Li, Minghui,Li, Puyu,Wang, Lin,Feng, Mengyuan,Han, Lijun,Li, Minghui,Wang, Lin.

[10]Multi-Residue Method for the Screening of Benzimidazole and Metabolite Residues in the Muscle and Liver of Sheep and Cattle Using HPLC/PDAD with DVB-NVP-SO3Na for Sample Treatment. Xiong, Lin,Shimo, Shimo Peter,Li, Weihong,Yang, Xiaolin,Yan, Ping,Xiong, Lin,Shimo, Shimo Peter,Li, Weihong,Yang, Xiaolin,Yan, Ping,Huang, Lele.

[11]Efficient Coproduction of Mannanase and Cellulase by the Transformation of a Codon-Optimized Endomannanase Gene from &ITAspergillus niger&IT into &ITTrichoderma reesei &IT. Sun, Xianhua,Xue, Xianli,Li, Mengzhu,Gao, Fei,Hao, Zhenzhen,Huang, Huoqing,Luo, Huiying,Yao, Bin,Su, Xiaoyun,Qin, Lina. 2017

[12]Effect of dietary fatty acids on serum parameters, fatty acid compositions, and liver histology in Shaoxing laying ducks. Liu, Wei-meng,Lu, Li-zhi,Zhang, Jing,Tao, Zheng-rong,Shen, Jun-da,Li, Guo-qin,Wang, De-qian,Li, Jin-jun,Tian, Yong,Liu, Wei-meng,Lai, Shu-jing,Shi, Fang-xiong,Zhang, Jing,Liu, Yu,Yu, Bo. 2011

[13]Effectiveness of a 95 SNP panel for the screening of breed label fraud in the Chinese meat market. Rogberg-Munoz, A.,Ripoli, M. V.,Carino, M. H.,Liron, J. P.,Peral-Garcia, P.,Giovambattista, G.,Rogberg-Munoz, A.,Wei, S.,Guo, B. L.,Wei, Y. M.,Prando, A. J.,Vaca, R. J. A..

[14]Invited review: mesenchymal progenitor cells in intramuscular connective tissue development. Miao, Z. G.,Miao, Z. G.,Zhang, L. P.,Fu, X.,Yang, Q. Y.,Dodson, M. V.,Du, M.,Zhang, L. P.,Zhu, M. J..

[15]Relationship Between Protein Denaturation and Water Holding Capacity of Pork During Postmortem Ageing. Li, Xia,Wei, Xiuli,Wang, Hang,Zhang, Chun-hui,Mehmood, Waris. 2018

[16]Association of LXRA gene variants with carcass and meat quality traits in beef cattle. Gan, Qianfu,Xu, Shangzhong,Gan, Qianfu,Zhang, Lupei,Xu, Shangzhong,Li, Hengde,Li, Junya,Gao, Xue,Ren, Hongyan,Chen, Jinbao. 2008

[17]Different actions of salt and pyrophosphate on protein extraction from myofibrils reveal the mechanism controlling myosin dissociation. Shen, Qingwu W.,Shen, Qingwu W.,Wang, Zhenyu,Liu, Yue,Gao, Yuan,Zhang, Dequan,Swartz, Darl R..

[18]Using near infrared spectroscopy to predict the physical traits of Bos grunniens meat. Zhang, Li,Sun, Baozhong,Xie, Peng,Li, Haipeng,Su, Huawei,Sha, Kun,Huang, Caixia,Lei, Yuanhua,Liu, Xuan,Wang, Huan.

[19]Foreign meat identification by DNA breed assignment for the Chinese market. Rogberg-Munoz, A.,Ripoli, M. V.,Carino, M. H.,Castillo, N.,Villegas Castagnaso, E. E.,Liron, J. P.,Morales Durand, H. F.,Peral-Garcia, P.,Giovambattista, G.,Wei, S.,Guo, B. L.,Wei, Y. M.,Melucci, L.,Villarreal, E..

[20]Quantitative Analysis of 10 Mycotoxins in Wheat Flour by Ultrahigh Performance Liquid Chromatography-Tandem Mass Spectrometry with a Modified QuEChERS Strategy. Zhou, Qingxin,Li, Fenghua,Chen, Leilei,Jiang, Dafeng,Li, Fenghua,Jiang, Dafeng. 2016

作者其他论文 更多>>

微信小程序