Rapid residue analysis of oxathiapiprolin and its metabolites in typical Chinese soil, water, and sediments by a modified quick, easy, cheap, effective, rugged, and safe method with ultra high performance liquid chromatography and tandem mass spectrometry

文献类型： 外文期刊

第一作者： Ju, Chao

作者： Ju, Chao;Dong, Fengshou;Liu, Xingang;Wu, Xiaohu;Zhao, Huanhuan;Zheng, Yongquan;Xu, Jun

作者机构：

关键词： Metabolites;Oxathiapiprolin;Sediment;Soil;Water

期刊名称：JOURNAL OF SEPARATION SCIENCE （ 影响因子：3.645； 五年影响因子：2.943 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A sensitive and effective method for the simultaneous determination of residues from a new fungicide, oxathiapiprolin, and its metabolites (IN-E8S72 and IN-WR791) in soil, water, and sediment, was developed using ultra high performance liquid chromatography with tandem mass spectrometry. Three compounds were extracted from water, soil, and sediment by using acetonitrile and different proportions of formic acid aqueous solution (1% v/v for water; 2% v/v for soil; and sediment), and were cleaned with octadecylsilane. The target compounds were determined within 5 min using an electrospray ionization source in the positive mode for oxathiapiprolin and in the negative mode for the two metabolites. The limits of quantification for all the three compounds were 0.1 mu g/kg in water and 1 mu g/kg in soil and sediment. Recovery studies were performed using three spiked levels (0.1, 1, and 10 mu g/kg for water; 1, 10, and 50 mu g/kg for soil and sediment). The overall average recoveries ranged from 64.8 to 112.7% with all intra-and interday relative standard deviation values below 19.4 and 19.1%, respectively. The method validation confirmed that the proposed method was convenient and reliable for determining residual oxathiapiprolin and its metabolites in soil, water, and sediments.

分类号： O6

  • 相关文献

[1]Simultaneous determination of oxathiapiprolin and two metabolites in fruits, vegetables and cereal using a modified quick, easy, cheap, effective, rugged, and safe method and liquid chromatography coupled to tandem mass spectrometry. Xu, Jun,Dong, Fengshou,Liu, Xingang,Li, Yuanbo,Zheng, Yongquan. 2014

[2]Influence of a heavy rainfall event on the leaching of [C-14]isoproturon and its degradation products in outdoor lysimeters. Doerfler, Ulrike,Cao, Guoyin,Grundmann, Sabine,Schroll, Reiner.

[3]Forest runoff increase mercury output from subtropical forest catchments: an example from an alpine reservoir in a national nature reserve (southwestern China). Ma, Ming,Wang, Dingyong,Sun, Tao,Zhao, Zheng,Ma, Ming,Wang, Dingyong,Sun, Tao,Zhao, Zheng,Du, Hongxia.

[4]A statistical approach to determine fluxapyroxad and its three metabolites in soils, sediment and sludge based on a combination of chemometric tools and a modified quick, easy, cheap, effective, rugged and safe method. Liu, Xingang,Zhu, Yulong,Dong, Fengshou,Xu, Jun,Zheng, Yongquan,Li, Minmin.

[5]Multi-element pollution in soil, ground and surface water from abandoned chromate chemical plants: a case study in Hangzhou, China. Zou, Lina,Wang, Shaoxian,Hashmi, Muhammad Z.,Tang, Xianjin,Shi, Jiyan,Wang, Shaoxian,Liu, Lei,Liu, Lei. 2015

[6]Determination of Herbicide Propisochlor in Soil, Water and Rice by Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Method Using by UPLC-ESI-MS/MS. Xu, Jun,Liu, Xingang,Dong, Fengshou,Zheng, Yongquan,Wu, Yanbing,Zhang, Ying.

[7]Rapid residue analysis of four triazolopyrimidine herbicides in soil, water, and wheat by ultra-performance liquid chromatography coupled to tandem mass spectrometry. Liu, Xingang,Xu, Jun,Li, Yuanbo,Dong, Fengshou,Li, Jing,Zheng, Yongquan,Song, Wenchen.

[8]Enantioselective separation of the carfentrazone-ethyl enantiomers in soil, water and wheat by HPLC. Dong, Fengshou,Liu, Xingang,Xu, Jun,Chen, Wuying,Cheng, Li,Ning, Ping,Li, Jing,Zheng, Yongquan,Wang, Yunhao.

[9]Transmission Efficiency of Cucumber green mottle mosaic virus via Seeds, Soil, Pruning and Irrigation Water. Li, Jun-Xiang,Liu, Shan-Shan,Gu, Qin-Sheng.

[10]Enantioseparation and Determination of the Chiral Fungicide Furametpyr Enantiomers in Rice, Soil, and Water by High-Performance Liquid Chromatography. Chen, Xiu,Xu, Jun,Liu, Xingang,Chen, Zenglong,Li, Yuanbo,Zheng, Yongquan,Zhang, Hongjun.

[11]Petroleum contamination of soil and water, and their effects on vegetables by statistically analyzing entire data set. Zhang, Juan,Du, Xiao-ming,Li, Fa-sheng,Hou, Hong,Yang, Jun-cheng,Fan, Shu-kai.

[12]Development of a multi-residue enantiomeric analysis method for 9 pesticides in soil and water by chiral liquid chromatography/tandem mass spectrometry. Dong, Fengshou,Liu, Xingang,Xu, Jun,Chen, Xiu,Han, Yongtao,Liang, Xuyang,Zheng, Yongquan.

[13]Atmospheric pressure gas chromatography quadrupole-time-of-flight mass spectrometry for simultaneous determination of fifteen organochlorine pesticides in soil and water. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wu, Xiaohu,Chen, Zenglong,Pan, Xinglu,Zheng, Yongquan.

[14]Simultaneous measurements of cations and anions using diffusive gradients in thin films with a ZrO-Chelex mixed binding layer. Wang, Yan,Ding, Shiming,Shi, Lei,Gong, Mengdan,Xu, Shiwei,Zhang, Chaosheng.

[15]Dissipation of chlorpyrifos and residue analysis in rice, soil and water under paddy field conditions. Zhang, Xiao,Shen, Yan,Yu, Xiang-yang,Liu, Xian-jin,Zhang, Xiao.

[16]Determination of oxathiapiprolin concentration and dissipation in grapes and soil by ultrahigh-performance liquid chromatography-tandem mass spectrometry. Yu, Pingzhong,Jia, Chunhong,Zhao, Ercheng,Chen, Li,Jing, Junjie,He, Min,He, Hongju.

[17]Activity of the novel fungicide oxathiapiprolin against plant-pathogenic oomycetes. Miao, Jianqiang,Dong, Xue,Lin, Dong,Wang, Qiushi,Liu, Pengfei,Liu, Xili,Chen, Furu,Du, Yixin.

[18]Earthworms enhanced winter oilseed rape (Brassica napus L.) growth and nitrogen uptake. Zhang, Shujie,Chao, Ying,Zhang, Chunlei,Cheng, Jing,Li, Jun,Ma, Ni.

[19]N, P Contribution and soil adaptability of four arbuscular mycorrhizal fungi. Wenke, Liu.

[20]Protective function of narrow grass hedges on soil and water loss on sloping croplands in Northern China. Xiao, Bo,Wang, Qing-hai,Wu, Ju-ying,Huang, Chuan-wei,Yu, Ding-fang,Xiao, Bo.

作者其他论文 更多>>

微信小程序