Determination of Ochratoxin A in Pig Kidneys by Immunoaffinity Cleanup and Ultra-High Performance Liquid Chromatography

文献类型： 外文期刊

第一作者： Hou, YaLi

作者： Hou, YaLi;Lv, FengLin;Hou, YaLi;Li, YuPing;Xie, JiangHua;Zhou, Li;Zhou, Jinhui

作者机构：

期刊名称：JOURNAL OF AOAC INTERNATIONAL （ 影响因子：1.913； 五年影响因子：1.754 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： An accurate method was developed for determining ochratoxin A (OTA) in pig kidney using an immunoaffinity column for cleanup and ultra-HPLC/MS/MS for identification and quantification. Mean recoveries of OTA from kidney samples fortified at 0.10-5 mu g/kg levels ranged from 74 to 92%, with RSDs of 4.6-7.5%. The LOD was estimated to be 0.03 mu g/kg and the LOQ was 0.10 mu g/kg based on an S/N in kidney of 3:1 and 10:1, respectively. The developed method was used for the determination of OTA in pig kidney. A survey of the OTA content of pig kidneys slaughtered in Chongqing, China, revealed that 35 out of 40 analyzed samples were contaminated; the OTA concentration in kidney ranged from trace level (0.03-0.1) to 0.323 mu g/kg. This method was shown to be useful for accurately evaluating the intake of OTA from pig kidneys.

分类号： O65

  • 相关文献
作者其他论文 更多>>
  • Integrative omics analyses of tea (Camellia sinensis) under glufosinate stress reveal defense mechanisms: A trade-off with flavor loss

    作者：Yu, Huan;Miao, Peijuan;Zhou, Chunran;Cheng, Haiyan;Dong, Qinyong;Pan, Canping;Li, Dong;Wu, Yangliu;Zhao, Yingjie;Liu, Zhusheng;Zhao, Yingjie;Zhou, Li

    关键词：Tea; Glufosinate; Transcriptome; Metabolomic; Quality

  • CRISPR/Cas9 revolutionizes Macleaya cordata breeding: a leap in sanguinarine biosynthesis

    作者：Sun, Mengshan;Liu, Wei;Zeng, Jianguo;Sun, Mengshan;Zhou, Li;Song, Rong;Sun, Mengshan;Zhong, Xiaohong;Liu, Wei;Zeng, Jianguo;Huang, Peng;Zeng, Jianguo

    关键词：

  • Insight into the fate of tolfenpyrad in tea plant (Camellia sinensis L.) from root uptake

    作者：Wang, Zihan;Wang, Xinru;Li, Ziqiang;Wang, Min;Fan, Wenwen;Zha, Chengmin;Zhou, Li;Zhang, Xinzhong;Chen, Zongmao;Luo, Fengjian;Wang, Xinru;Zhou, Li;Zhang, Xinzhong;Chen, Zongmao;Luo, Fengjian

    关键词：Tolfenpyrad; Tea plant; Root uptake; Transport; Metabolism; Distribution

  • Identification of aggregation pheromones released by the stick tea thrips (Dendrothrips minowai) larvae and their application for controlling thrips in tea plantations

    作者：Cai, Xiaoming;Chen, Zongmao;Xiu, Chunli;Zhang, Fengge;Luo, Zongxiu;Bian, Lei;Li, Zhaoqun;Fu, Nanxia;Zhou, Li;Magsi, Fida Hussain;Cai, Xiaoming;Chen, Zongmao;Pan, Hongsheng;Xiu, Chunli;Luo, Zongxiu;Bian, Lei;Li, Zhaoqun;Fu, Nanxia;Zhou, Li;Magsi, Fida Hussain;Cai, Xiaoming;Chen, Zongmao;Zhang, Fengge

    关键词：Dendrothrips minowai; aggregation pheromone; electrophysiological and behavioral responses; field trapping

  • Climate-shaped vegetation dominated the spatial pattern of the Bowen ratio over terrestrial ecosystems in China

    作者：Sun, Mingyu;Han, Lang;Yao, Yuan;Wang, Jilong;Yu, Guirui;Chen, Zhi;Hao, Tianxiang;Yang, Meng;Zhang, Weikang;Liu, Zhaogang;Ma, Lexin;Dou, Xiaojun;Luo, Wenxing;Lin, Yong;He, Yongtao;Shi, Peili;Wang, Huimin;Zhang, Yangjian;Zhao, Fenghua;Zhu, Zhilin;Yu, Guirui;Chen, Zhi;Liu, Zhaogang;Ma, Lexin;Dou, Xiaojun;Luo, Wenxing;Lin, Yong;He, Yongtao;Shi, Peili;Zhang, Yangjian;Chen, Zhi;Zhu, Xianjin;Han, Lang;Chen, Shiping;Deng, Zhengmiao;Duh, Hu;Wei, Wenxue;Dong, Gang;Gao, Yanhong;Ji, Xibin;Li, Yuqiang;Tan, Junlei;Gu, Fengxue;Hao, Xiangxiang;Hao, Yanbin;Hen, Qihua;He, Jinsheng;He, Jinsheng;He, Jinsheng;He, Jinsheng;Chen, Shiping;Jiang, Zhengde;Wu, Jiabing;Zhu, Jiaojun;Li, Xinhu;Li, Yingnian;Zhao, Liang;Li, Yuzhe;Zhang, Fawei;Liu, Shaomin;Luo, Weijun;Mo, Xingguo;Zhang, Yiping;Sha, Liqing;Song, Qinghai;Zhang, Yiping;Sun, Dan;Yan, Junhua;Tan, Junlei;Tang, Yakun;Wang, Fei;Wang, Jianlin;Wu, Zhixiang;Xin, Xiaoping;Xin, Xiaoping;Zhang, Yucui;Zhou, Li;Zhang, Weikang;Chen, Zhi

    关键词：Bowen ratio; Heat flux; Sensible heat; Eddy covariance; Spatial patterns; Energy partitioning

  • A ratiometric fluorescence and colorimetry dual-signal sensing strategy based on o-phenylenediamine and AuNCs for determination of Cu2+ and glyphosate

    作者：Li, Ziqiang;Zhang, Changsheng;Zhou, Li;Luo, Fengjian;Lou, Zhengyun;Chen, Zongmao;Zhang, Xinzhong;Yang, Mei;Li, Ziqiang;Zhang, Changsheng;Zhou, Li;Luo, Fengjian;Lou, Zhengyun;Chen, Zongmao;Zhang, Xinzhong;Yang, Mei;Liang, Shuang;Zhang, Changsheng

    关键词：Fluorescence detection; Visual sensing; GSH-AuNCs; Cu2+; Glyphosate

  • A compendium of genetic regulatory effects across pig tissues

    作者：Teng, Jinyan;Gao, Yahui;Xu, Zhiting;Lin, Qing;Diao, Shuqi;Pan, Xiangchun;Wei, Chen;Zhang, Zhe;Zhang, Zhe;Gao, Yahui;Li, Cong-jun;Liu, George E.;Gao, Yahui;Gao, Yahui;Yin, Hongwei;Bai, Lijing;Yang, Liu;Yi, Guoqiang;Tang, Zhonglin;Li, Kui;Yin, Hongwei;Bai, Zhonghao;Bai, Zhonghao;Yu, Xiaoshan;Haley, Chris;Navarro, Pau;Tenesa, Albert;Fang, Lingzhao;Liu, Shuli;Zhao, Bingru;Yang, Wenjing;Ding, Xiangdong;Li, Xiujin;Pan, Zhangyuan;Yang, Wenjing;Guan, Dailu;Pan, Zhangyuan;Hou, Yali;Hou, Yali;Keel, Brittney N.;Rohrer, Gary A.;Lindholm-Perry, Amanda K.;Oliver, William T.;Ballester, Maria;Crespo-Piazuelo, Daniel;Quintanilla, Raquel;Rawlik, Konrad;Xia, Charley;Xia, Charley;Yao, Yuelin;Yao, Wenye;Karlskov-Mortensen, Peter;Fredholm, Merete;Amills, Marcel;Clop, Alex;Amills, Marcel;Godia, Marta;Clop, Alex;Giuffra, Elisabetta;Rocha, Dominique;Wang, Sheng;Rocha, Dominique;Dekkers, Jack C. M.;Kramer, Luke;Tuggle, Christopher K.;Corbett, Ryan;Charles, Mathieu;Pausch, Hubert;Hu, Xiaoxiang;Frantz, Laurent;Frantz, Laurent;Luo, Yonglun;Lin, Lin;Luo, Yonglun;Lin, Lin;Luo, Yonglun;Zhang, Zhe;Chen, Zitao;Cui, Leilei;Cui, Leilei;Cui, Leilei;Cui, Leilei;Cui, Leilei;Xiang, Ruidong;Xiang, Ruidong;Shen, Xia;Shen, Xia;Shen, Xia;Li, Pinghua;Huang, Ruihua;Tang, Guoqing;Li, Mingzhou;Zhao, Yunxiang;Jiang, Jicai;Yuan, Xiaolong;Liu, Xiaohong;Zhao, Shuhong;Zhao, Pengju;Zhao, Shuhong;Zhao, Pengju;Zhao, Pengju;Haley, Chris;Tenesa, Albert;Zhang, Qin;Tenesa, Albert

    关键词：

微信小程序