Synthesis of Isotopically Labeled C-13(3)-Simazine and Development of a Simultaneous UPLC-MS/MS Method for the Analysis of Simazine in Soil

文献类型： 外文期刊

第一作者： Guo, Yangzhen

作者： Guo, Yangzhen;Zhang, Xia;Yang, Yue;Chen, Shuo;She, Dongmei;Song, Yan;Zhang, Xia;Yang, Yue;She, Gaimei

作者机构：

关键词： C-13(3)-simazine;synthesis;IDMS;UPLC-MS;MS;isotope labelling

期刊名称：MOLECULES （ 影响因子：4.411； 五年影响因子：4.587 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： The isotope dilution mass spectrometry (IDMS) is a highly efficient method for tackling the ion suppression in complex matrix by ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS), but a lack of commercial internal standards is a limiting factor for these analyses. Herein, an economical and efficient strategy for the synthesis of C-13(3)-simazine via a three-step procedure was developed. The isotope-labeled internal standard was used for determination of simazine residue in soil samples. The quantitation method has a limit of detection of 0.015 g/kg and quantitation of 0.08 g/kg. The inter-day and intra-day precision of the method were below 4.6%. Recovery values were ranged between 92.9% and 99.2%. All the samples obtained from six provinces in China contained from 1 to 62 g/kg of simazine.

分类号： O62

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