Simultaneous determination of flupyradifurone and its two metabolites in fruits, vegetables, and grains by a modified quick, easy, cheap, effective, rugged, and safe method using ultra high performance liquid chromatography with tandem mass spectrometry

文献类型: 外文期刊

第一作者: Liu, Xingang

作者: Liu, Xingang;Wu, Xiaohu;Dong, Fengshou;Xu, Jun;Zheng, Yongquan

作者机构:

关键词: Flupyradifurone;Injection solvents;Metabolites;Tandem mass spectrometry;Ultra high performance liquid chromatography

期刊名称:JOURNAL OF SEPARATION SCIENCE ( 影响因子:3.645; 五年影响因子:2.943 )

ISSN:

年卷期:

页码:

收录情况: SCI

摘要: An effective analytical method for the simultaneous determination of a novel insecticide flupyradifurone and its two metabolites was developed using ultra high performance liquid chromatography with tandem mass spectrometry coupled with a quick, easy, cheap, effective, rugged, and safe procedure. The three target compounds were extracted with acetonitrile and cleaned up with octadecylsilane, and were separated successfully between 1.9 and 3.1 min using an HSS T3 chromatographic column connected to an electrospray ionization source. All the matrix-matched samples at three fortified levels (0.01, 0.05, and 0.5 mg/kg) provided satisfactory recoveries in the range of 70.3-116.5% with relative standard deviations below 18.6%. The limits of quantitation were 10 g/kg for flupyradifurone and difluoroethylamino-furanone and 100 g/kg for 6-chloronicotinic acid. The limit of quantification of flupyradifurone was far below the maximum residue limit in the USA. The method is of great significance for establishing maximum residue limits in China.

分类号: O6

  • 相关文献

[1]Performance comparison of dispersive solid-phase extraction and multiplug filtration cleanup methods for the determination of tefuryltrione in plant and environmental samples using UHPLC-MS/MS. Yu, Yang,Ji, Mingshan,Tao, Yan,Dong, Fengshou,Xu, Jun,Liu, Xingang,Wu, Xiaohu,Zheng, Yongquan. 2017

[2]Determination of five sulfonylurea herbicides in environmental waters and soil by ultra high performance liquid chromatography with tandem mass spectrometry after extraction using graphene. Li, Cheng,Lu, Anxiang,Wang, Jihua,Ping, Hua,Luan, Yunxia,Chen, Jiayi,Lu, Anxiang,Li, Jie,Ha, Xuejiao.

[3]Simultaneous determination of pyrifluquinazon and its main metabolite in fruits and vegetables by using QuEChERS-HPLC-MS/MS. You, Xiangwei,Sui, Chengcheng,Li, Yiqiang,Wang, Xiuguo.

[4]Multi-mycotoxins analysis in raw milk by ultra high performance liquid chromatography coupled to quadrupole orbitrap mass spectrometry. Zheng, Nan,Wen, Fang,Wang, Jiaqi,Mao, Jianfei,Zheng, Nan,Wen, Fang,Wang, Jiaqi,Mao, Jianfei,Zheng, Nan,Wen, Fang,Wang, Jiaqi,Mao, Jianfei,Guo, Lingan,Fu, Chengping,Ouyang, Huaxue,Zhong, Lingli,Lei, Shaorong,Mao, Jianfei,Guo, Lingan,Fu, Chengping,Ouyang, Huaxue,Zhong, Lingli,Lei, Shaorong. 2018

[5]Determination of Phenylethanolamine A in Animal Feeds Using Ultra High Performance Liquid Chromatography-Photodiode Array Detector. Wang Rui-Guo,Su Xiao-Ou,Wang Pei-Long,Li Yang,Fan Yu-Fei. 2013

[6]Simultaneous determination of trifloxystrobin and trifloxystrobin acid residue in rice and soil by a modified quick, easy, cheap, effective, rugged, and safe method using ultra high performance liquid chromatography with tandem mass spectrometry. Xu, Jun,Liu, Xingang,Tao, Yan,Pan, Xinglu,Zheng, Yongquan,Dong, Fengshou. 2014

[7]Simultaneous determination of three herbicides in wheat, wheat straw, and soil using a quick, easy, cheap, effective, rugged, and safe method with ultra high performance liquid chromatography and tandem mass spectrometry. Xu, Jun,Dong, Fengshou,Liu, Xingang,Wu, Xiaohu,Zheng, Yongquan,Zhao, Huanhuan,Wu, Yanbing.

[8]Detection of 13 mycotoxins in feed using modified QuEChERS with dispersive magnetic materials and UHPLC-MS/MS. Qian, Mingrong,Yang, Hua,Wang, Jianmei,Ji, Xiaofeng,Xu, Jie,Li, Zuguang,Liu, Yanping,Wu, Huizhen. 2018

[9]Determination of neonicotinoid insecticides residues in eels using subcritical water extraction and ultra-performance liquid chromatography-tandem mass spectrometry. Xiao, Zhiming,Yang, Yunxia,Li, Yang,Fan, Xia,Ding, Shuangying.

[10]Towards posttranslational modification proteome of royal jelly. Zhang, Lan,Fang, Yu,Li, Rongli,Feng, Mao,Han, Bin,Zhou, Tiane,Li, Jianke.

[11]Proteomic analysis of Fasciola hepatica excretory and secretory products (FhESPs) involved in interacting with host PBMCs and cytokines by shotgun LC-MS/MS. Liu, Qing,Huang, Si-Yang,Yue, Dong-Mei,Wang, Jin-Lei,Zhu, Xing-Quan,Liu, Qing,Wang, Yujian,Li, Xiangrui,Huang, Si-Yang,Zhu, Xing-Quan.

[12]Magnetic molecularly imprinted polymers for the determination of beta-agonist residues in milk by ultra high performance liquid chromatography with tandem mass spectrometry. Liu, Hongcheng,Lin, Xin,Lin, Tao,Luo, Yinglan,Li, Qiwan,Liu, Hongcheng,Lin, Xin,Lin, Tao,Luo, Yinglan,Li, Qiwan,Liu, Hongcheng,Lin, Xin,Lin, Tao,Luo, Yinglan,Li, Qiwan,Zhang, Yulong.

[13]Simultaneous determination of Ltx and Ltxd in cured meat products by LC/MS/MS. Song, Hui,Wu, Haihong,Geng, Zhiming,Sun, Chong,Ren, Shuang,Wang, Daoying,Zhang, Muhan,Liu, Fang,Xu, Weimin,Song, Hui,Ren, Shuang,Xu, Weimin.

[14]Global and quantitative proteomic analysis of dogs infected by avian-like H3N2 canine influenza virus. Su, Shuo,Hong, Malin,Zhou, Pei,Lu, Gang,Zhang, Guihong,Li, Shoujun,Su, Shuo,Hong, Malin,Zhou, Pei,Lu, Gang,Li, Shoujun,Tian, Jin,Zhu, Huachen,Zhu, Huachen,Lai, Alexander. 2015

[15]Comparison of different cleanup procedures for oil crops based on the development of a trace analytical method for the determination of pyraclostrobin and epoxiconazole. Dong, Fengshou,Xu, Jun,Liu, Xingang,Cheng, Youpu,Chen, Zenglong,Liu, Na,Chen, Xixi,Tao, Yan,Zheng, Yongquan.

[16]Enantioselective separation and pharmacokinetic dissipation of cyflumetofen in field soil by ultra-performance convergence chromatography with tandem mass spectrometry. Dong, Fengshou,Xu, Jun,Liu, Xingang,Chen, Zenglong,Pan, Xinglu,Chen, Xixi,Zheng, Yongquan,Liu, Na.

[17]Comprehensive identification of novel proteins and N-glycosylation sites in royal jelly. Zhang, Lan,Han, Bin,Li, Rongli,Lu, Xiaoshan,Fang, Yu,Feng, Mao,Li, Jianke,Zhang, Lan,Lu, Xiaoshan,Nie, Aiying,Guo, Lihai. 2014

[18]Comparative proteomics of leaves found at different stem positions of maize seedlings. Chen, Yi-Bo,Zhao, Biligen-Gaowa,Wang, Bai-Chen,Wang, Dan,Wang, Xu-Chu,Ge, Xuan-Liang.

[19]Simultaneous Determination of 13-HODE, 9,10-DHODE, and 9,10,13-THODE in Cured Meat Products by LC-MS/MS. Song, Hui,Wu, Haihong,Geng, Zhiming,Sun, Chong,Ren, Shuang,Wang, Daoying,Zhang, Muhan,Liu, Fang,Xu, Weimin,Song, Hui,Ren, Shuang,Xu, Weimin.

[20]Simultaneous determination of florfenicol with its metabolite based on modified quick, easy, cheap, effective, rugged, and safe sample pretreatment and evaluation of their degradation behavior in agricultural soils. Xu, Mingfei,Qian, Mingrong,Zhang, Hu,Wang, Jianmei,Wu, Huizhen,Ma, Junwei.

作者其他论文 更多>>