Iron (II, III) oxide/multi-walled carbon nanotube composite as solid-phase extraction sorbent followed by ultra-high performance liquid chromatography tandem mass spectrometry for simultaneous determination of zearalenone and type A trichothecenes in Salviae miltiorrhizae Radix et Rhizoma (Danshen)

文献类型: 外文期刊

第一作者: Jiang, Keqiu

作者: Jiang, Keqiu;Huang, Peng;Luan, Lianjun;Wu, Yongjiang;Fan, Kai;Guo, Wenbo;Zhao, Zhihui;Han, Zheng

作者机构:

关键词: Salviae miltiorrhiza Radix et Rhizoma;Zearalenone;Type A trichothecenes;Solid-phase extraction;Iron (II;III) oxide/multi-walled carbon nanotube composite;Ultra-high performance liquid;chromatography-tandem mass spectrometry

期刊名称:JOURNAL OF CHROMATOGRAPHY A ( 影响因子:4.759; 五年影响因子:4.302 )

ISSN:

年卷期:

页码:

收录情况: SCI

摘要: For the first time, a reliable solid-phase extraction (SPE) procedure using iron (II, III) oxide (Fe3O4)/multi-walled carbon nanotube (MWCNT) composite as sorbents was proposed for purification and enrichment of zearalenone (ZEA) and four type A trichothecenes (T-2 toxin (T-2), HT-2 toxin (HT-2), neosolaniol (NEO) and diacetoxyscirpenol (DAS)) in Salviae miltiorrhiza Radix et Rhizoma (Danshen). The Fe3O4/MWCNT composite was synthesized by assembling Fe3O4 with MWCNT by sonication through an "aggregation wrap" mechanism and several key parameters affecting the performance of SPE procedure such as the composition of sample loading solutions, washing and elution solvents were thoroughly investigated. After optimization, 2% acetonitrile aqueous solution as the loading solution, 5% methanol aqueous solution as the washing solution and acetone containing 0.5% formic acid as the elution solvent presented an excellent purification efficiency for the five targets in Danshen. Under the optimal sample pretreatment conditions followed by analysis with ultra-high performance liquid chromatography-tandem mass spectrometry, satisfactory linearity (R-2 >= 0.991), high sensitivity (limit of quantification in the range of 1.20-4.80 mu g kg(-1)), good recovery (73.7-91.9%) and acceptable precision (RSD, 2.1-13.3%) were obtained. The applicability of the validated method was further verified in real Salviae miltiorrhiza Radix et Rhizoma samples. (C) 2016 Elsevier B.V. All rights reserved.

分类号: O65

  • 相关文献

[1]Multi-walled carbon nanotubes as solid-phase extraction sorbents for simultaneous determination of type A trichothecenes in maize, wheat and rice by ultra-high performance liquid chromatography-tandem mass spectrometry. Dong, Maofeng,Si, Wenshuai,Nie, Dongxia,Zhao, Zhihui,Han, Zheng,De Saeger, Sarah,Han, Zheng,Jiang, Keqiu,Wu, Yongjiang.

[2]Determination of type A trichothecenes in coix seed by magnetic solid-phase extraction based on magnetic multi-walled carbon nanotubes coupled with ultra-high performance liquid chromatography-tandem mass spectrometry. Dong, Maofeng,Si, Wenshuai,Wang, Weimin,Bai, Bing,Nie, Dongxia,Song, Weiguo,Zhao, Zhihui,Han, Zheng,Guo, Yirong,Han, Zheng.

[3]Cloning, expression of a peroxiredoxin gene from Acinetobacter sp SM04 and characterization of its recombinant protein for zearalenone detoxification. Yu, Yuanshan,Wu, Hui,Yu, Yuanshan,Wu, Hui,Tang, Yuqian,Qiu, Liping. 2012

[4]Biological detoxification of zearalenone by Aspergillus niger strain FS10. Sun, Xiulan,He, Xingxing,Li, Yun,Qian, He,Li, Yun,Xu, Dan,Xue, Kathy Siyu. 2014

[5]The Mycotoxin Zearalenone Hinders Candida albicans Biofilm Formation and Hyphal Morphogenesis. Rajasekharan, Satish Kumar,Lee, Jin-Hyung,Lee, Jintae,Zhao, Yueju. 2018

[6]Rapid detection and quantification of zearalenone-producing Fusarium species by targeting the zearalenone synthase gene PKS4. Meng, Kun,Wang, Yaru,Yang, Peilong,Luo, Huiying,Bai, Yingguo,Shi, Pengjun,Yuan, Tiezheng,Ma, Rui,Yao, Bin. 2010

[7]Secretory expression and characterization of a novel peroxiredoxin for zearalenone detoxification in Saccharomyces cerevisiae. Wu, Hui,Yu, Yuanshan. 2013

[8]The Antagonistic Effect of Mycotoxins Deoxynivalenol and Zearalenone on Metabolic Profiling in Serum and Liver of Mice. Ji, Jian,Cui, Fangchao,Pi, Fuwei,Zhang, Yinzhi,Li, Yun,Wang, Jiasheng,Sun, Xiulan,Zhu, Pei,Ji, Jian,Zhu, Pei,Cui, Fangchao,Pi, Fuwei,Zhang, Yinzhi,Sun, Xiulan,Li, Yun,Wang, Jiasheng. 2017

[9]Screening and monitoring zearalenone-producing Fusarium species by PCR and zearalenone by monoclonal antibodies in feed from China. Pei, Shi-Chun,Zhang, Hong-Fu,Ji, Cheng,Pei, Shi-Chun,Zhen, Yu-Ping,Gao, Jian-Wei,Lee, Won-Jong,Chen, Cong,Zhang, Xuan-Zhe.

[10]Recent mycotoxin survey data and advanced mycotoxin detection techniques reported from China: a review. Selvaraj, Jonathan Nimal,Wang, Yan,Zhou, Lu,Zhao, Yueju,Xing, Fuguo,Dai, Xiaofeng,Liu, Yang.

[11]A novel detoxifying agent: Using rice husk carriers to immobilize zearalenone-degrading enzyme from Aspergillus niger FS10. He, Mengling,Li, Yun,Pi, Fuwei,Ji, Jian,He, Xingxing,Zhang, Yinzhi,Sun, Xiulan,Li, Yun.

[12]Individual and combined cytotoxicity assessment of zearalenone with ochratoxin A or alpha-zearalenol by full factorial design. Zheng, N.,Gao, Y. N.,Wang, H. W.,Wang, J. Q.,Zheng, N.,Gao, Y. N.,Wang, J. Q.,Wang, H. W.,Liu, J.. 2018

[13]Mycotoxin detection - Recent trends at global level. Selvaraj, Jonathan Nimal,Zhou Lu,Wang Yan,Zhao Yue-ju,Xing Fu-guo,Dai Xiao-feng,Liu Yang. 2015

[14]Rapid and sensitive quantitation of zearalenone in food and feed by lateral flow immunoassay. Liu, Gang,Han, Zheng,Nie, Dongxia,Yang, Junhua,Zhao, Zhihui,Song, Suquan,Wu, Aibo,Liu, Gang,Zhang, Jingbo,Li, Heping,Liao, Yucai,Song, Suquan,De Saeger, Sarah. 2012

[15]Metabolic Profile of Zearalenone in Liver Microsomes from Different Species and Its in Vivo Metabolism in Rats and Chickens Using Ultra High-Pressure Liquid Chromatography-Quadrupole/Time-of-Flight Mass Spectrometry. Yang, Shupeng,Zhang, Jinzhen,Jin, Yue,Zhou, Jinhui,Li, Yi,Yang, Shupeng,Zhang, Huiyan,De Ruyck, Karl,De Saeger, Sarah,De Boevre, Marthe,Yang, Shupeng,Zhang, Huiyan,Sun, Feifei,Wang, Zhanhui,Zhang, Suxia,Li, Yanshen. 2017

[16]Effects of aflatoxin B1 combined with ochratoxin A and/or zearalenone on metabolism, immune function, and antioxidant status in lactating dairy goats. Huang, Shuai,Fan, Caiyun,Wang, Shang,Cheng, Jianbo,Zheng, Nan,Jabar, Adil,Wang, Jiaqi,Cheng, Ming. 2018

[17]Multi-component immunochromatographic assay for simultaneous detection of aflatoxin B-1, ochratoxin A and zearalenone in agro-food. Li, Xin,Li, Peiwu,Zhang, Qi,Li, Ran,Zhang, Wen,Zhang, Zhaowei,Ding, Xiaoxia,Tang, Xiaoqian,Li, Xin,Zhang, Qi,Li, Ran,Zhang, Zhaowei,Li, Xin,Li, Peiwu,Li, Peiwu,Zhang, Zhaowei,Ding, Xiaoxia,Li, Peiwu,Zhang, Qi,Li, Ran,Zhang, Wen,Tang, Xiaoqian. 2013

[18]Evaluation of reduced toxicity of zearalenone as measured by the Hep G2 cell assay on degradation enzymes. He, Xingxing,Li, Yun,Gu, Wenshu,Sun, Yange,Sun, Xiulan,Li, Shuai,Li, Yun.

[19]Occurrence of mycotoxins in feed ingredients and complete feeds obtained from the Beijing region of China. Zhao, Lihong,Fan, Yu,Ma, Shanshan,Ji, Cheng,Ma, Qiugang,Zhang, Jianyun,Jia, Yaxiong,Sun, Lei.

[20]Cytotoxicity induced by ochratoxin A, zearalenone, and alpha-zearalenol: Effects of individual and combined treatment. Wang, H. W.,Wang, J. Q.,Li, S. L.,Zhang, Y. D.,Zheng, N.,Wang, H. W.,Li, F. D.,Wang, H. W.,Wang, J. Q.,Li, S. L.,Zhang, Y. D.,Zheng, N.,Zheng, B. Q.. 2014

作者其他论文 更多>>