Multi-pesticides residue analysis of grains using modified magnetic nanoparticle adsorbent for facile and efficient cleanup

文献类型： 外文期刊

第一作者： Liu, Zhenzhen

作者： Liu, Zhenzhen;Qi, Peipei;Wang, Xiangyun;Wang, Zhiwei;Xu, Xiahong;Zhang, Hu;Wang, Qiang;Wang, Xinquan;Liu, Zhenzhen;Chen, Wenxue;Wang, Qiang;Qi, Peipei;Wang, Xiangyun;Wang, Qiang;Qi, Peipei;Wang, Xiangyun;Wang, Zhiwei;Xu, Xiahong;Zhang, Hu;Wang, Xinquan;Wang, Zhiwei;Xu, Xiahong;Zhang, Hu;Wang, Xinquan

作者机构：

关键词： Fe3O4-PSA;Grain;Multi-pesticides residue;LC-MS/MS

期刊名称：FOOD CHEMISTRY （ 影响因子：7.514； 五年影响因子：7.516 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A facile, rapid sample pretreatment method was developed based on magnetic nanoparticles for multi pesticides residue analysis of grains. Magnetite (Fe3O4) nanoparticles modified with 3-(N,N-diethyla mino)propyltrimethoxysilane (Fe3O4-PSA) and commercial C18 were selected as the cleanup adsorbents to remove the target interferences of the matrix, such as fatty acids and non-polar compounds. Rice was used as the representative grain sample for method optimization. The amount of Fe3O4-PSA and C18 were systematically investigated for selecting the suitable purification conditions, and the simultaneous determination of 50 pesticides and 8 related metabolites in rice was established by liquid chromatography tandem mass spectrometry. Under the optimal conditions, the method validation was performed including linearity, sensitivity, matrix effect, recovery and precision, which all satisfy the requirement for pesticides residue analysis. Compared to the conventional QuEChERS method with non-magnetic material as cleanup adsorbent, the present method can save 30% of the pretreatment time, giving the high throughput analysis possible. (C) 2017 Elsevier Ltd. All rights reserved.

分类号： TS2`TS201.2

  • 相关文献

[1]Identification of quantitative trait locus of zinc and phosphorus density in wheat (Triticum aestivum L.) grain. Shi, Rongli,Zhang, Fusuo,Zou, Chunqin,Li, Hongwei,Tong, Yiping,Jing, Ruilian.

[2]An efficient cleanup method coupled with gas chromatography and mass spectrometry for multi-pesticides residue analysis in complex plant matrices. Wang, Xinquan,Qi, Peipei,Wang, Xiangyun,Zhang, Qian,Wang, Zhiwei,Xu, Xiahong,Xu, Hao,Zhang, Hu,Wang, Qiang,Wang, Xinquan,Xu, Xiahong,Xu, Hao,Zhang, Hu,Wang, Qiang,Wang, Xinquan,Qi, Peipei,Wang, Xiangyun,Zhang, Qian,Wang, Zhiwei,Xu, Xiahong,Xu, Hao,Zhang, Hu,Wang, Qiang,Qi, Peipei,Wang, Xiangyun,Zhang, Qian,Wang, Zhiwei.

[3]Mineral element concentrations in grains of Chinese wheat cultivars. Yong Zhang,Qichao Song,Jun Yan,Jianwei Tang,Rongrong Zhao,Yueqiang Zhang,Zhonghu He,Chunqin Zou,Ivan Ortiz-Monasterio. 2010

[4]Zinc biofortification of wheat through fertilizer applications in different locations of China. Zhang, Yue-Qiang,Karim, Md. Rezaul,Xue, Yan-Fang,Yan, Peng,Meng, Qing-Feng,Cui, Zhen-Ling,Zhang, Fu-Suo,Zou, Chun-Qin,Sun, Yi-Xiang,Ye, You-Liang,Cakmak, Ismail. 2012

[5]Cultivar differences in photosynthetic tolerance to photooxidation and shading in rice (Oryza sativa L.). Jiao, DM,Li, X. 2001

[6]Cadmium and lead contamination in japonica rice grains and its variation among the different locations in southeast China. Cheng, FM,Zhao, NC,Xu, HM,Li, Y,Zhang, WF,Zhu, ZW,Chen, MX. 2006

[7]Study on Near-Infrared Spectroscopy Signal Pre-processing and Model Building. Zhang Xiaochao,Zhang Yinqiao,Wang Hui. 2009

[8]Arsenic Distribution, Species, and Its Effect on Maize Growth Treated with Arsenate. Ci Xiao-ke,Liu Hua-lin,Hao Yu-bo,Zhang Ji-wang,Liu Peng,Dong Shu-ting,Liu Hua-lin,Ci Xiao-ke. 2012

[9]Characteristics and influencing factors of grass-feeding livestock breeding in China: An economic geographical perspective. Wang Guogang,Wang Mingli,Wang Jimin,Yang Chun,Liu Yufeng. 2016

[10]Determination of Abamectin Residues in Grain by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. He Hong-Mei,Zhao Hua,Zhang Chun-Rong,Zhu Ya-Hong,Ping Li-Feng,Wu Min,Zhang Chang-Peng,Cai Xiao-Ming,Li Zhen. 2013

[11]Interspecific complementary and competitive interactions between intercropped maize and faba bean. Li, L,Yang, SC,Li, XL,Zhang, FS,Christie, P.

[12]Coupled Effects of Soil Water and Nutrients on Growth and Yields of Maize Plants in a Semi-Arid Region. Sun Zhan-Xiang,Zheng Jia-Ming,Sun Wen-Tao.

[13]Comparative proteomic analyses of two Taxus species (Taxus X media and Taxus mairei) reveals variations in the metabolisms associated with paclitaxel and other metabolites. Juan Hao,Shen, Chenjia,Hong Guo,Xinai Shi,Ye Wang,Qinghua Wan,Yao-Bin Song,Lei Zhang,Ming Dong,Chenjia Shen. 2017

[14]Validated LC-MS/MS method for determination of YH-8, a novel PKnB inhibitor, in rat plasma and its application to pharmacokinetic study. Zhai, Qianqian,Pang, Jing,Li, Guoqing,Li, Congran,Yang, Xinyi,Yu, Liyan,Wang, Yucheng,You, Xuefu,Zhai, Qianqian,Pang, Jing,Li, Guoqing,Li, Congran,Yang, Xinyi,Yu, Liyan,Wang, Yucheng,You, Xuefu,Zhai, Qianqian,Li, Jian. 2015

[15]A method for multiple identification of four beta(2)-Agonists in goat muscle and beef muscle meats using LC-MS/MS based on deproteinization by adjusting pH and SPE for sample cleanup. Xiong, Lin,Gao, Ya-Qin,Li, Wei-Hong,Guo, Tian-Feng,Yang, Xiao-Lin,Xiong, Lin,Gao, Ya-Qin,Li, Wei-Hong,Guo, Tian-Feng,Yang, Xiao-Lin. 2015

[16]Development and Validation of a Liquid Chromatography-Tandem Mass Spectrometry Method Coupled with Dispersive Solid-Phase Extraction for Simultaneous Quantification of Eight Paralytic Shellfish Poisoning Toxins in Shellfish. Yang, Xianli,Zhao, Zhiyong,Nie, Dongxia,Zhou, Changyan,Zhou, Lei,Shi, Xizhi,Tan, Yanglan,Liu, Hong. 2017

[17]Serum Metabolic Profiling of Oocyst-Induced Toxoplasma gondii Acute and Chronic Infections in Mice Using Mass-Spectrometry. Zhou, Chun-Xue,Chen, Xiao-Qing,Zhu, Xing-Quan,Zhou, Chun-Xue,He, Shen-Yi,Cong, Wei,Chen, Xiao-Qing,Elsheikha, Hany M.. 2018

[18]Validated hydrophilic interaction LC-MS/MS method for determination of N-methyl-2-pyrrolidinone residue. Applied to a depletion study of N-methyl-2-pyrrolidinone in swine liver following intramuscular administration of drug N-methyl-2-pyrrolidinone formulation. Liu, Yanhong,Ji, Yanhong,Chen, Jingtao,Chen, Ximing,Wang, Guangxiang,Shang, Youjun,Liu, Xiangtao,Pan, Jack. 2010

[19]Simultaneous analysis of cyromazine, sulfonamides and tetracyclines in animal wastewater and soil samples by optimized LC-MS/MS. Wei, Ruicheng. 2012

[20]Investigation of metabolites accumulation in medical plant Gentiana rigescens during different growing stage using LC-MS/MS and FT-IR. Pan, Yu,Zhang, Ji,Zhao, Yan-Li,Wang, Yuan-Zhong,Pan, Yu,Huang, Heng-Yu. 2015

作者其他论文 更多>>

微信小程序