Determination of Polybrominated Diphenyl Ethers and Derivatives, Tetrabromobisphenol A, Hexabromocyclododecane in Egg Samples by Gel Permeation Chromatography and Dispersive Solid Phase Extraction

文献类型： 外文期刊

第一作者： Li Min-Jie

作者： Li Min-Jie;Jin Fen;Yang Li-Li;Wu Ri-Na;Shao Hua;Jin Mao-Jun;Wang Jing

作者机构：

关键词： Polybrominated diphenyl ethers and derivatives;Tetrabromobisphenol A;Hexabromocyclododecane;Egg;Gel permeation chromatography;Dispersive solid phase extraction

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2014 年 42 卷 9 期

页码：

收录情况： SCI

摘要： A stimulate method for determination of polybrominated diphenyl ethers (PBDEs) and derivatives (OH-PBDEs and MeO-PBDEs), tetrabromobisphenol A (TBBPA), hexabromocyclododecane (HBCD) in egg samples was developed by gel permeation chromatography (GPC) and dispersive solid phase extraction (DSPE) combined with liquid chromatography tandem mass spectrometric (HPLC-MS/MS) and gas chromatography-negative chemical ionization mass spectrometry (GC-NCI/MS). The analytes were extracted with mixture of hexane and dichloromethane (1:1, V/V) by accelerated solvent extraction (ASE), and purified by 100 mg C-18 dispersive solid phase extraction (SPE) sorbents followed with gel permeation chromatography (GPC), and then analyzed by liquid chromatography tandem mass spectrometric (HPLC-MS/MS) and gas chromatography-negative chemical ionization mass spectrometry (GC-NCI/MS), respectively. The quantitation was carried out external standard method. The recoveries of objects were 64.5% - 97.2% and 65.6% - 109.2% (except BDE85 was 54.8%, OH-BDE-137 was 47.4%) spiked at 1.0 mu g/kg or 5.0 mu g/kg in egg white and egg yolk, respectively. The relative standard deviations (RSDs) were less than 20.2%. The limits of quantitation (LOQ) for the object were 0.01 - 0.2 mu g/kg.

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