Simultaneous Determination of 3 Kinds of Isomers of Clorprenaline and Baclofen Residues in Feed by Ultra Performance Liquid Chromatography-Tandem Mass spectrometry

文献类型： 外文期刊

第一作者： Li Yang

作者： Li Yang;Su Xiao-Ou;Wang Pei-Long;Fan Xia;Wang Rui-Guo;Wang Xiao

作者机构：

关键词： Feed;Clorprenaline;Isomer;Baclofen;Ultra performance liquid chromatography-tandem mass spectrometry

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2014 年 42 卷 4 期

页码：

收录情况： SCI

摘要： A sensitive method was developed for the determination of 3 kinds isomers of clorprenaline and baclofen residues in feed by solvent extraction combined with solid-phase extraction pretreatment and ultra performance liquid chromatography-tandem mass spectrometry. The sample was extracted for 20 min under shaking by the mixed solution of 0. 1 moUL formic solution and acetonitrile (4: 1, V/V), separated under centrifuging to eliminate impurity, and cleaned up by MCX cartridge. The test potion was separated by waters BEH C-18 columns with gradient elution program. Analyte confirmation was performed using multiple reaction monitoring ( MRM) with one precursor ion and productions as identifiers. The results were calculated by external standard method. The LODs were 20 mu g/Kg, LOQs were 50 tig/Kg, the recoveries were in range of 80% 110%, and the relative standard deviation ( RSDs) were less than or equal to 10. 2% at three spiked levels.

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