Simultaneous determination of cyflumetofen and its main metabolite residues in samples of plant and animal origin using multi-walled carbon nanotubes in dispersive solid-phase extraction and ultrahigh performance liquid chromatography-tandem mass spectrometry

文献类型: 外文期刊

第一作者: Liu, Xingang

作者: Liu, Xingang;Dong, Fengshou;Xu, Jun;Li, Yuanbo;Zheng, Yongquan;Li, Minmin;Kong, Zhiqiang

作者机构:

关键词: Cyflumetofen;Metabolites;WMCNTs;Plant origin;Animal origin;UPLC-MS/MS

期刊名称:JOURNAL OF CHROMATOGRAPHY A ( 影响因子:4.759; 五年影响因子:4.302 )

ISSN: 0021-9673

年卷期: 2013 年 1300 卷

页码:

收录情况: SCI

摘要: A rapid and effective method for the simultaneous determination of cyflumetofen and its main metabolite residues in samples of plant and animal origin (tomato, apple, eggplant, soybean, green tea, fish, and pork liver) was developed using ultrahigh performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). Samples were extracted with acetonitrile and cleaned-up with multi-walled carbon nanotubes (MWCNTs). The determination of the presence of target compounds was achieved in less than 4.0 min using an electrospray ionization source in the positive mode (ESI+) for cyflumetofen and 2-(trifluoromethyl) benzamide (B-3) and the negative mode (ESI-) for alpha,alpha,alpha-trifluoro-o-toluic acid (B-1). The entire method was validated by evaluating the repeatability, linearity, precision, trueness, and matrix effect. Average recoveries of the analytes were in the range of 79.3-117.6% with relative standard deviation values below 7.6%. Limits of quantification (LOQs) ranged from 0.7 to 9.8 mu g kg(-1), which were lower than the maximum residue limits (MRLs) for the cyflumetofen found in foods in Japan. (C) 2013 Elsevier B.V. All rights reserved.

分类号:

  • 相关文献

[1]Degradation of cyflumetofen and formation of its main metabolites in soils and water/sediment systems. Liu, Xingang,Xu, Jun,Dong, Fengshou,Wu, Xiaohu,Zheng, Yongquan,Li, Minmin. 2016

[2]Effective Monitoring of Fluxapyroxad and Its Three Biologically Active Metabolites in Vegetables, Fruits, and Cereals by Optimized QuEChERS Treatment Based on UPLC-MS/MS. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wu, Xiaohu,Zheng, Yongquan.

[3]Simultaneous determination of three pesticides and their metabolites in unprocessed foods using ultraperformance liquid chromatography-tandem mass spectrometry. Wu, Xiaohu,Xu, Jun,Dong, Fengshou,Liu, Xingang,Pan, Xinglu,Du, Pengqiang,Wei, Dongmei,Zheng, Yongquan,Rong, Lili,Zheng, Yongquan. 2018

[4]Simultaneous determination of 14 antiviral drugs and relevant metabolites in chicken muscle by UPLC-MS/MS after QuEChERS preparation. Qian, Yongzhong,Qiu, Jing.

[5]Simultaneous determination of oxathiapiprolin and two metabolites in fruits, vegetables and cereal using a modified quick, easy, cheap, effective, rugged, and safe method and liquid chromatography coupled to tandem mass spectrometry. Xu, Jun,Dong, Fengshou,Liu, Xingang,Li, Yuanbo,Zheng, Yongquan. 2014

[6]Enantioselective separation and pharmacokinetic dissipation of cyflumetofen in field soil by ultra-performance convergence chromatography with tandem mass spectrometry. Dong, Fengshou,Xu, Jun,Liu, Xingang,Chen, Zenglong,Pan, Xinglu,Chen, Xixi,Zheng, Yongquan,Liu, Na.

[7]Distribution behaviour of acaricide cyflumetofen in tomato during home canning. Dong, Fengshou,Chen, Zenglong,Xu, Jun,Liu, Xingang,Zheng, Yongquan,Liu, Na,Duan, Lifang,Li, Minmin.

[8]Chiral determination of a novel acaricide cyflumetofen enantiomers in cucumber, tomato, and apple by HPLC. Dong, Fengshou,Liu, Xingang,Xu, Jun,Li, Jing,Li, Yuanbo,Li, Minmin,Zheng, Yongquan,Wang, Yunhao.

[9]Determination of virginiamycin M1 residue in tissues of swine and chicken by ultra-performance liquid chromatography tandem mass spectrometry. Wang, Xiaoyang,Wang, Mi,Zhang, Keyu,Hou, Ting,Zhang, Lifang,Fei, Chenzong,Xue, Feiqun,Wang, Xiaoyang,Hang, Taijun. 2018

[10]Rapid Determination of Organonitrogen, Organophosphorus and Carbamate Pesticides in Tea by Ultrahigh-Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS). Zhao, Hong-Xia,Yang, Guo-Sheng,Zhao, Shan-Cang,Deng, Li-Gang,Mao, Jiang-Sheng,Guo, Chang-Ying,Lu, Xiao,Zhao, Shan-Cang,Deng, Li-Gang,Mao, Jiang-Sheng,Guo, Chang-Ying,Lu, Xiao,Zhao, Shan-Cang,Deng, Li-Gang,Mao, Jiang-Sheng,Guo, Chang-Ying,Lu, Xiao,Aboul-Enein, Hassan Y.. 2013

[11]Determination of difenoconazole residue in tomato during home canning by UPLC-MS/MS. Dong, Fengshou,Xu, Jun,Liu, Xingang,Li, Jing,Li, Yuanbo,Chen, Xiu,Zheng, Yongquan,Zhang, Changpeng,Shan, Weili. 2012

[12]Transformation of deoxynivalenol and its acetylated derivatives in Chinese steamed bread making, as affected by pH, yeast, and steaming time. Wang, Bujun.

[13]Determination of Herbicide Propisochlor in Soil, Water and Rice by Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Method Using by UPLC-ESI-MS/MS. Xu, Jun,Liu, Xingang,Dong, Fengshou,Zheng, Yongquan,Wu, Yanbing,Zhang, Ying.

[14]Validation of a confirmatory method of salbutamol in sheep hair by UPLC-MS/MS and its application to pharmacokinetic study. Suo Decheng,Zhang Wei,Zhang Yu,Zhao Genlong,Wang Ruigou,Wang PeiLong,Su Xiaoou.

[15]Determination of chlorantraniliprole residues in corn and soil by UPLC-ESI-MS/MS and its application to a pharmacokinetic study. Xu, Jun,Liu, Xingang,Li, Jing,Li, Yuanbo,Kong, Zhiqiang,Zheng, Yongquan,Shan, Weili,Zheng, Zuntao.

[16]Quantitative multiresidue analysis of antibiotics in milk and milk powder by ultra-performance liquid chromatography coupled to tandem quadrupole mass spectrometry. Tian, He,Wang, Jiaqi,Zhang, Yangdong,Li, Songli,Zheng, Nan,Jiang, Jindou,Tao, Dali.

[17]Determination of imidacloprid residues in Chinese Cabbage by UPLC-MS/MS. Zha, Yubing,Huang, Maofang,Yang, Chunliang,Wang, Mingyue,Wang, Xiaofang,Lin, Ling,Zeng, Shaodong,Zha, Yubing,Yang, Chunliang,Wang, Mingyue,Wang, Xiaofang,Lin, Ling,Zeng, Shaodong,Liu, Jianxing. 2014

[18]The effects of ferulic acid on the pharmacokinetics of warfarin in rats after biliary drainage. Wang, Yang,Fan, Rong,Tang, Tao,Luo, Jiekun,Xia, Zian,Li, Haigang,Lv, Huiying,Sun, Hua,Xie, Haitang. 2016

[19]Method for determination of streptomycin and streptidine as markers for streptomycin industrial dregs monitoring in pig and poultry compound feeds. Li, Yang,Peng, Qing,Qiao, Yu,Shi, Bo,Li, Yang,Su, Xiaoou.

[20]Miniaturized liquid-liquid extraction coupled with ultra-performance liquid chromatography/tandem mass spectrometry for determination of topramezone in soil, corn, wheat, and water. Dong, Fengshou,Liu, Xingang,Xu, Jun,Li, Jing,Lu, Caihong,Zheng, Yongquan,Wang, Yunhao.

作者其他论文 更多>>