Determination of Prothioconazole and Prothioconazole-desthio in Peanut Samples by Liquid Chromatography-Tandem Mass Spectrometry

文献类型： 外文期刊

第一作者： Shi Xiao-Mei

作者： Shi Xiao-Mei;Jin Fen;Du Xin-Wei;Huang Yu-Ting;Wang Miao;Wang Jing;Jin Mao-Jun;Shao Hua

作者机构：

关键词： High performance liquid chromatography tandem mass spectrometry;Peanut;Prothioconazole;Prothioconazole-desthio

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2012 年 40 卷 8 期

页码：

收录情况： SCI

摘要： A sensitive method was developed for determination of prothioconazole and prothioconazole-desthio in peanut. The analytes were extracted from the peanut samples by acetonitril, and defatted with n-hexane saturated by acetonitrile. Then the samples were purified by dispersion solid phase extraction using ODS C-18 sorbent, and analyzed by liquid chromatography tandem mass spectrometry (LC-MS/MS). Prothioconazole and prothioconazole-desthio were separated on a reversed phase column using a gradient elution program of aqueous solution containing 5 mmol/L ammonium acetate and 0.2% acetic acid (A) and acetonitrile solution (B). Analyte confirmation was performed using multiple reaction monitoring (MRM) with one precursor ion and two productions as identifiers. The recoveries were in the range of 87.2%-102.46%, and the relative standard deviation (RSDs) were less than 9.97% at 2.0, 4.0, and 20.0 mu g/kg three spiked levels for prothioconazole and prothioconazole-desthio. The limits of quantification (LOQ) for the two analytes were 2.0 mu g/kg.

分类号：

  • 相关文献

[1]Simultaneous Determination of 5 Peptide Antibiotics in Bovine Milk Samples by Liquid Chromatography-Tandem Mass Spectrometry. Liu Jia-Jia,Jin Fen,She Yong-Xin,Liu Hong-Bin,Shi Xiao-Mei,Wang Miao,Wang Jing,Xu Si-Yuan. 2011

[2]Determination of Glucocorticoids in Muscle Tissues by Liquid Chromatography-Electrospray Tandem Mass Spectrometry. Gong Lan,Chen Ming,Wei Xian,Zou Chun,Wang Ran. 2016

[3]Transgenic Expression and Identification of Recombinant Human Proinsulin in Peanut. Zheng Ling,Wang Yu,Wan Shu-Bo,Peng Zhen-Ying,Bi Yu-Ping,Zheng Ling,Wang Yu,Bian Fei,Wan Shu-Bo,Peng Zhen-Ying,Zheng Ling,Wang Yu,Bian Fei,Wan Shu-Bo,Peng Zhen-Ying,Bi Yu-Ping,Jiao Qi-Qing,Qu Shu-Jie,Wan Shu-Bo,Bi Yu-Ping. 2016

[4]Transcriptome Analysis of Calcium and Hormone-Related Gene Expressions during Different Stages of Peanut Pod Development. Li, Yan,Meng, Jingjing,Yang, Sha,Guo, Feng,Zhang, Jialei,Geng, Yun,Cui, Li,Li, Xinguo,Wan, Shubo. 2017

[5]Calcium contributes to photoprotection and repair of photosystem II in peanut leaves during heat and high irradiance. Yang, Sha,Wang, Fang,Guo, Feng,Meng, Jing-Jing,Li, Xin-Guo,Yang, Sha,Guo, Feng,Meng, Jing-Jing,Li, Xin-Guo,Wan, Shu-Bo,Wang, Fang. 2015

[6]Cloning of Acyl-ACP thioesterase FatA from Arachis hypogaea L. and its expression in Escherichia coli. Chen, G.,Peng, Z. Y.,Xuan, N.,Zhang, Y.,Bi, Y. P.,Chen, G.. 2012

[7]Genome-Wide Identification and Comparative Analysis of Cytosine-5 DNA Methyltransferase and Demethylase Families in Wild and Cultivated Peanut. Wang, Pengfei,Gao, Chao,Bian, Xiaotong,Zhao, Shuzhen,Zhao, Chuanzhi,Xia, Han,Song, Hui,Hou, Lei,Wan, Shubo,Wang, Xingjun. 2016

[8]Peanut (Arachis hypogaea L.) Omics and Biotechnology in China. Wang, Xing-Jun,Xia, Han,Wan, Shu-Bo,Zhao, Chuan-Zhi,Li, Ai-Qin,Wang, Xing-Jun,Xia, Han,Wan, Shu-Bo,Zhao, Chuan-Zhi,Li, Ai-Qin,Wang, Xing-Jun,Xia, Han,Wan, Shu-Bo,Zhao, Chuan-Zhi,Li, Ai-Qin,Liu, Shuan-Tao. 2011

[9]Identification of Metabolites and Transcripts Involved in Salt Stress and Recovery in Peanut. Cui, Feng,Liu, Yiyang,Han, Yan,Wan, Shubo,Li, Guowei,Cui, Feng,Liu, Yiyang,Han, Yan,Wan, Shubo,Li, Guowei,Sui, Na,Liu, Shanshan,Duan, Guangyou. 2018

[10]Small RNA profiling and degradome analysis reveal regulation of microRNA in peanut embryogenesis and early pod development. Gao, Chao,Wang, Pengfei,Zhao, Shuzhen,Zhao, Chuanzhi,Xia, Han,Hou, Lei,Zhang, Ye,Li, Changsheng,Wang, Xingjun,Wang, Xingjun,Ju, Zheng. 2017

[11]Genome-Wide Dissection of the Heat Shock Transcription Factor Family Genes in Arachis. Wang, Pengfei,Song, Hui,Li, Changsheng,Li, Pengcheng,Li, Aiqin,Guan, Hongshan,Hou, Lei,Wang, Xingjun,Wang, Xingjun. 2017

[12]Identification and expression dynamics of three WUSCHEL related homeobox 13 (WOX13) genes in peanut. Wang, Pengfei,Li, Changsheng,Li, Cui,Zhao, Chuanzhi,Xia, Han,Zhao, Shuzhen,Hou, Lei,Gao, Chao,Wan, Shubo,Wang, Xingjun,Wang, Pengfei,Li, Changsheng,Li, Cui,Zhao, Chuanzhi,Xia, Han,Zhao, Shuzhen,Hou, Lei,Gao, Chao,Wan, Shubo,Wang, Xingjun.

[13]Comparative proteomics of peanut gynophore development under dark and mechanical stimulation. Sun, Yong,Wang, Qingguo,Li, Zhen,Hou, Lei,Liu, Wei,Dai, Shaojun,Sun, Yong.

[14]Transcriptome and Differential Expression Profiling Analysis of the Mechanism of Ca2+ Regulation in Peanut (Arachis hypogaea) Pod Development. Yang, Sha,Zhang, Jialei,Geng, Yun,Guo, Feng,Meng, Jingjing,Li, Xinguo,Li, Lin,Wang, Jianguo,Sui, Na,Wan, Shubo. 2017

[15]Identification of chilling-responsive transcripts in peanut (Arachis hypogaea L.). Wang, Chuan Tang,Wang, Xiu Zhen,Chi, Xiao Yuan,Wu, Qi,Chen, Dian Xu,Tang, Yue Yi,Yang, Guan Pin,Feng, Tong,Gao, Hua Yuan,Xu, Ya Long. 2011

[16]Physiological fundamentals of the AnM cultivation technique in peanut production: Leaf photosynthetic hysteresis is reduced by exposing hypocotyls. Qin, Feifei,Takano, Tetsuo,Qin, Feifei,Xu, Hui-lian,Qin, Feifei. 2012

[17]Functional Genomic Analysis of Aspergillus flavus Interacting with Resistant and Susceptible Peanut. Wang, Houmiao,Lei, Yong,Yan, Liying,Wan, Liyun,Ren, Xiaoping,Chen, Silong,Jiang, Huifang,Liao, Boshou,Wang, Houmiao,Lei, Yong,Yan, Liying,Wan, Liyun,Ren, Xiaoping,Chen, Silong,Jiang, Huifang,Liao, Boshou,Dai, Xiaofeng,Guo, Wei. 2016

[18]The effect of low water content on seed longevity. Hu, CL,Zhang, YL,Tao, M,Hu, XR,Jiang, CY. 1998

[19]Identification and Evaluation of Single-Nucleotide Polymorphisms in Allotetraploid Peanut (Arachis hypogaea L.) Based on Amplicon Sequencing Combined with High Resolution Melting (HRM) Analysis. Hong, Yanbin,Liu, Ying,Chen, Xiaoping,Liang, Xuanqiang,Hong, Yanbin,Huang, Shangzhi,Pandey, Manish K.,Varshney, Rajeev K.,Liu, Hong,Varshney, Rajeev K.,Varshney, Rajeev K.. 2015

[20]Identification of QTLs associated with oil content and mapping FAD2 genes and their relative contribution to oil quality in peanut (Arachis hypogaea L.). Pandey, Manish K.,Qiao, Lixian,Feng, Suping,Khera, Pawan,Wang, Hui,Guo, Baozhu,Pandey, Manish K.,Khera, Pawan,Varshney, Rajeev K.,Pandey, Manish K.,Qiao, Lixian,Feng, Suping,Khera, Pawan,Wang, Hui,Culbreath, Albert K.,Guo, Baozhu,Wang, Ming Li,Tonnis, Brandon,Barkley, Noelle A.,Qiao, Lixian,Feng, Suping,Wang, Hui,Wang, Jianping,Holbrook, C. Corley. 2014

作者其他论文 更多>>

微信小程序