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Determination of androstenone levels in porcine plasma by LC-MS/MS

文献类型：外文期刊

第一作者： Chen, G.

作者： Chen, G.;Yang, S. M.;Qiu, J.;Ren, L.;Kamal-Eldin, A.;Lundstrom, K.

作者机构：

关键词： Androstenone;Porcine plasma;Solid-phase extraction;LC-MS/MS

期刊名称：FOOD CHEMISTRY （影响因子：7.514；五年影响因子：7.516 ）

ISSN： 0308-8146

年卷期： 2010 年 122 卷 4 期

页码：

收录情况： SCI

摘要： Androstenone (5 alpha-androst-16-en-3-one) is a major component in boar taint. Here, a liquid chromatography-tandem mass spectrometry method was developed to analyse androstenone in porcine plasma to facilitate studies of its transport from pig testes to adipose tissues. The method used androstanone (5 alpha-andro-stan-3-one) as internal standard, Oasis (R) MCX solid-phase extraction, C18 reversed-phase column, and API 5000 Triple Quadrupole mass spectrometry with positive electrospray ionisation interface operating in the multiple reaction monitoring mode. Incubation of the plasma samples with beta-glucuronidase/arylsulfatase revealed an increase in androstenone yield indicating the presence of a conjugated form of its 3-enol isomer. With this method the limit of detection (LOD) was 1.0 ng and the limit of quantification (LOQ) was 3.3 ng per mL of plasma. In conclusion, the presented method is sensitive and reproducible and thus suitable for accurate quantification of androstenone levels in a small volume of porcine plasma. (C) 2010 Elsevier Ltd. All rights reserved.

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