Magnetic solid-phase extraction based on graphene oxide for the determination of lignans in sesame oil

文献类型： 外文期刊

第一作者： Wu, Linxia

作者： Wu, Linxia;Yu, Li;Ding, Xiaoxia;Li, Peiwu;Dai, Xianhong;Chen, Xiaomei;Zhou, Haiyan;Bai, Yizhen;Ding, Jian;Yu, Li;Ding, Xiaoxia;Li, Peiwu;Chen, Xiaomei;Zhou, Haiyan;Bai, Yizhen;Wu, Linxia;Yu, Li;Ding, Xiaoxia;Li, Peiwu;Dai, Xianhong;Chen, Xiaomei;Ding, Jian;Wu, Linxia;Yu, Li;Ding, Xiaoxia;Li, Peiwu;Dai, Xianhong;Chen, Xiaomei;Ding, Xiaoxia;Li, Peiwu;Zhou, Haiyan;Bai, Yizhen;Ding, Jian

作者机构：

关键词： Magnetic solid-phase extraction;Sesamol;Sesamin;Sesamolin;High performance liquid chromatography

期刊名称：FOOD CHEMISTRY （ 影响因子：7.514； 五年影响因子：7.516 ）

ISSN： 0308-8146

年卷期： 2017 年 217 卷

页码：

收录情况： SCI

摘要： Graphene oxide was fabricated by a simple method and applied to magnetic solid-phase extraction. In a pretreatment procedure before the sesamol, sesamin and sesamolin in sesame oil were detected by high performance liquid chromatography. Several parameters affecting the extraction efficiency were investigated, including the type and volume of desorption solvent, desorption time and the amount of sorbent. Under the optimized conditions, the detection limits of sesamol, sesamin, and sesamolin were 0.05 mu g/g, 0.02 mu g/g, and 0.02 mu g/g, respectively. The limits of quantification were all 0.21 mu g/g. The average recoveries of sesamol, sesamin, and sesamolin were 84.55%, 85.47%, 86.83%, respectively and their relative standard deviations were 1.23%, 1.33%, and 0.84%, respectively. (C) 2016 Published by Elsevier Ltd.

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