QuEChERS Purification Combined with Ultrahigh-Performance Liquid Chromatography Tandem Mass Spectrometry for Simultaneous Quantification of 25 Mycotoxins in Cereals

文献类型: 外文期刊

第一作者: Sun, Juan

作者: Sun, Juan;Li, Weixi;Zhang, Yan;Hu, Xuexu;Wu, Li;Wang, Bujun;Sun, Juan;Li, Weixi;Zhang, Yan;Hu, Xuexu;Wu, Li;Wang, Bujun

作者机构:

关键词: ultrahigh performance liquid chromatography tandem mass spectrometry (UPLC-MS/MS);QuEChERS;mycotoxin;cereals

期刊名称:TOXINS ( 影响因子:4.546; 五年影响因子:4.8 )

ISSN: 2072-6651

年卷期: 2016 年 8 卷 12 期

页码:

收录情况: SCI

摘要: A method based on the QuEChERS (quick, easy, cheap, effective, rugged, and safe) purification combined with ultrahigh performance liquid chromatography tandem mass spectrometry (UPLC-MS/MS), was optimized for the simultaneous quantification of 25 mycotoxins in cereals. Samples were extracted with a solution containing 80% acetonitrile and 0.1% formic acid, and purified with QuEChERS before being separated by a C18 column. The mass spectrometry was conducted by using positive electrospray ionization (ESI+) and multiple reaction monitoring (MRM) models. The method gave good linear relations with regression coefficients ranging from 0.9950 to 0.9999. The detection limits ranged from 0.03 to 15.0 mu g.kg(-1), and the average recovery at three different concentrations ranged from 60.2% to 115.8%, with relative standard deviations (RSD%) varying from 0.7% to 19.6% for the 25 mycotoxins. The method is simple, rapid, accurate, and an improvement compared with the existing methods published so far.

分类号:

  • 相关文献

[1]A quick, easy, cheap, effective, rugged, and safe method for the simultaneous detection of four triazolone herbicides in cereals combined with ultrahigh performance liquid chromatography with tandem mass spectrometry. Tao, Yan,Xu, Jun,Liu, Xingang,Cheng, Youpu,Liu, Na,Chen, Zenglong,Dong, Fengshou,Zheng, Yonguan.

[2]On-farm conservation of 12 cereal crops among 15 ethnic groups in Yunnan (PR China). Xu, Furong,A, Xinxiang,Zhang, Feifei,Zhang, Enlai,Tang, Cuifeng,Dong, Chao,Yang, Yayun,Dai, Luyuan,Xu, Furong,A, Xinxiang,Zhang, Feifei,Zhang, Enlai,Tang, Cuifeng,Dong, Chao,Yang, Yayun,Dai, Luyuan,Xu, Furong,A, Xinxiang,Zhang, Feifei,Zhang, Enlai,Tang, Cuifeng,Dong, Chao,Yang, Yayun,Dai, Luyuan,Xu, Furong,A, Xinxiang,Zhang, Feifei,Zhang, Enlai,Tang, Cuifeng,Dong, Chao,Yang, Yayun,Dai, Luyuan,Liu, Xu.

[3]Rice ragged stunt oryzavirus: role of the viral spike protein in transmission by the insect vector. Zhou, GY,Lu, XB,Lu, HJ,Lei, JL,Chen, SX,Gong, ZX.

[4]Analysis of four sulfonylurea herbicides in cereals using modified Quick, Easy, Cheap, Effective, Rugged, and Safe sample preparation method coupled with liquid chromatography-tandem mass spectrometry. Ni, Yanxia,Yang, Huan,Zhang, Hantong,He, Qiao,Huang, Siqi,Qin, Meiling,Chai, Shuangshuang,Gao, Huanhuan,Ma, Youning. 2018

[5]Detoxification of gramine by the cereal aphid Sitobion avenae. Cai, Qing-Nian,Han, Ying,Hu, Yuan,Zhao, Xin,Cao, Ya-Zhong.

[6]Research of Heavy Metals Determination in Cereals by Inductively Coupled Plasma Mass Spectrometry. Wang Bu-jun. 2012

[7]Combination of dispersive solid-phase extraction and salting-out homogeneous liquid-liquid extraction for the determination of organophosphorus pesticides in cereal grains. Jia, Chunhong,Zhu, Xiaodan,Zhao, Ercheng,He, Min,Chen, Li,Yu, Pingzhong,Jia, Chunhong,Zhu, Xiaodan,Wang, Jihua,Zhao, Ercheng,He, Min,Chen, Li,Yu, Pingzhong.

[8]Some characteristics of cool weather-tolerant rice varieties in Yunnan Province, China. Tanno, H,Xiong, JH,Dai, LY,Ye, CR.

[9]THE EFFECTS OF 2IP AND 2,4-D ON RICE CALLI DIFFERENTIATION. Zhu, YX,Ouyang, WJ,Li, Y,Chen, ZL.

[10]Crop acquisition of phosphorus, iron and zinc from soil in cereal/legume intercropping systems: a critical review. Xue, Yanfang,Xia, Haiyong,Xia, Haiyong,Zhang, Zheng,Christie, Peter,Li, Long,Tang, Caixian.

[11]Phage-borne peptidomimetics as immunochemical reagent in dot-immunoassay for mycotoxin zearalenone. He, Qing-hua,Xu, Yang,Li, Yan-ping,Huang, Zhi-bing,Zhang, Cun-zheng. 2014

[12]Recent Advances in Mycotoxin Determination for Food Monitoring via Microchip. Man, Yan,Liang, Gang,Li, An,Pan, Ligang,Man, Yan,Liang, Gang,Li, An,Pan, Ligang,Man, Yan,Liang, Gang,Li, An,Pan, Ligang. 2017

[13]Ustiloxin G, a New Cyclopeptide Mycotoxin from Rice False Smut Balls. Wang, Xiaohan,Wang, Jian,Lai, Daowan,Wang, Weixuan,Zhou, Ligang,Dai, Jungui,Dai, Jungui,Liu, Yang. 2017

[14]Advances in research of nephrotoxicity and toxic antagonism of ochratoxin A. Zhao, Tao,Shen, Xiao Li,Chen, Wenying,Liao, Xin,Yang, Jieyeqi,Zou, Yan,Wang, Yan,Fang, Cuilan. 2017

[15]An oligosorbent-based aptamer affinity column for selective extraction of aflatoxin B-2 prior to HPLC with fluorometric detection. Liu, Hongmei,Luan, Yunxia,Lu, Anxiang,Li, Bingru,Wang, JiHua,Yang, Meihua,Yang, Meihua. 2018

[16]Determination for major chemical contaminants in tea (Camellia sinensis) matrices: A review. Li, Xin,Zhang, Zhaowei,Li, Peiwu,Zhang, Qi,Zhang, Wen,Ding, Xiaoxia,Li, Xin,Zhang, Zhaowei,Li, Peiwu,Zhang, Qi,Ding, Xiaoxia,Li, Xin,Zhang, Zhaowei,Li, Peiwu,Zhang, Qi,Li, Peiwu,Zhang, Wen,Ding, Xiaoxia,Zhang, Wen,Ding, Xiaoxia.

[17]Bioactive Bis-naphtho-gamma-pyrones from Rice False Smut Pathogen Ustilaginoidea virens. Lu, Shiqiong,Sun, Weibo,Meng, Jiajia,Wang, Ali,Wang, Xiaohan,Tian, Jin,Fu, Xiaoxiang,Lai, Daowan,Zhou, Ligang,Dai, Jungui,Dai, Jungui,Liu, Yang.

[18]Visual and microplate detection of aflatoxin B2 based on NaCl-induced aggregation of aptamer-modified gold nanoparticles. Luan, Yunxia,Chen, Jiayi,Li, Cheng,Ping, Hua,Ma, Zhihong,Lu, Anxiang,Xie, Gang.

[19]Characterization of Phenolic Compounds from Early and Late Ripening Sweet Cherries and Their Antioxidant and Antifungal Activities. Wang, Meng,Jiang, Nan,Wang, Yao,Jiang, Dongmei,Feng, Xiaoyuan,Wang, Meng,Jiang, Nan,Wang, Yao,Jiang, Dongmei,Feng, Xiaoyuan.

[20]Evaluation of latex agglutination inhibition reaction test for rapid detection of aflatoxin B-1. Chen, Fusheng,Wang, Xiaohong,Chen, Fusheng,Ye, Yang,Wang, Ping,Chen, Fusheng,Wang, Xiaohong,Zhou, Youxiang. 2011

作者其他论文 更多>>