Separation of enantiomers by high performance liquid chromatography using derivants of L-proline as chiral mobile phase additives

文献类型： 外文期刊

第一作者： Chang Yinxia

作者： Chang Yinxia;Hou Zhilin;Li Qiwan;Gao Tianrong;Yuan Liming

作者机构：

关键词： N-dodecanoyl-L-proline;N-dodecanoyl-L-proline-3,5-dimethylanilide;high performance liquid chromatography;mobile phase addition

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2006 年 34 卷

页码：

收录情况： SCI

摘要： N-dodecanoyl-L-proline and N-dodecanoyl-L-proline-3, 5-dimethylanilide derived from L-proline were used as chiral mobile phase additives. Enantiomers were separated using hexane and isopropanol as mobile phase on a aminopropyl silica gel column by high performance liquid chromatography. The results show that the enantioselectivity of N-dodecanoyl-L-proline is better and eight enantiomers of the twelve enantiomers can be separated. The enantioselectivity of N-dodecanoyl-L-proline-3,5-dimethyl-anilide is also good, but the basic line fluctuates strongly due to containing benzene ring in its molecular structure.

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