Determination of herbicide residues in garlic by GC-MS

文献类型: 外文期刊

第一作者: Aboul-Enein, Hassan Y.

作者: Aboul-Enein, Hassan Y.;Chen, Zilei;Zhang, Hong;Wang, Wenbo;Ding, Ruiyan;Du, Hongxia;Li, Huidong;Chen, Zilei;Liu, Bing;Yang, Guosheng

作者机构:

关键词: gas chromatography-mass spectrometry;microwave sulfur removal;garlic;herbicide residues

期刊名称:CHROMATOGRAPHIA ( 影响因子:2.044; 五年影响因子:1.725 )

ISSN: 0009-5893

年卷期: 2007 年 66 卷 11-12 期

页码:

收录情况: SCI

摘要: A rapid multi-residue method has been developed for the determination of 16 herbicides in garlic. The analytical procedure is based on prior microwave heating prevention of the generation of sulfur-containing compounds. The garlic samples which had been pretreated were extracted with acetonitrile and cleaned up by solid-phase extraction. The herbicide residues were detected by gas chromatography-mass spectrometry with selected ion monitoring. The recoveries of 16 herbicides ranged from 69.0 to 105.4% with the relative standard deviations (RSD) below 10.1%. The limit of quantification (LOQ) ranged from 0.003 to 0.015 mg kg(-1).

分类号:

  • 相关文献

[1]Rapid propagation of virus-free garlics and a systematic scheme for seed garlic production. Xu, PW,Sun, HS,Sun, RJ,Yang, YJ,Zhang, DC. 1997

[2]Effects of selenium and sulfur on antioxidants and physiological parameters of garlic plants during senescence. Cheng Bo,Lian Hai-feng,Yu Xin-hui,Sun Ya-li,Sun Xiu-dong,Shi Qing-hua,Liu Shi-qi,Liu Ying-ying. 2016

[3]A preliminary study on genetic analysis and purity assessment of the garlic germplasm and seed bulbs by the "finger printing" technique. Xu, PW,Yang, CL,Qu, SS,Yang, CY. 2005

[4]Control of Powdery Mildew in Organic Greenhouse Melon Cultivation. Qin, F. F.,Xu, H. L.,Xu, Q. C.. 2011

[5]Diversity evaluation of morphological traits and allicin content in garlic (Allium sativum L.) from China. Wang, Haiping,Li, Xixiang,Shen, Di,Oiu, Yang,Song, Jiangping.

[6]Influence of pH, concentration and light on stability of allicin in garlic (Allium sativum L.) aqueous extract as measured by UPLC. Wang, Haiping,Li, Xixiang,Liu, Xinyan,Shen, Di,Qiu, Yang,Zhang, Xiaohui,Song, Jiangping.

[7]Quantitative Determination of Allicin in Allium sativum L. Bulbs by UPLC. Wang, Haiping,Li, Xixiang,Liu, Su,Jin, Song.

[8]Effect on garlic greening and thermal stability of 1-(2 '-hydroxybenzene-1 '-carboxy-ethyl) pyrrole. Wang, Dan,Zhao, Guanghua,Wang, Dan,Li, Xihong,Wang, Dan,Zhao, Xiaoyan,Zhao, Guanghua,Zhao, Guanghua. 2011

[9]Influence of Garlic Intercropping or Active Emitted Volatiles in Releasers on Aphid and Related Beneficial in Wheat Fields in China. Chen Ju-lian,Sun Jing-rui,Cheng Deng-fa,Zhou Hai-bo,Francis, Frederic,Haubruge, Eric,Liu Yong,Bragard, Claude. 2013

[10]Impact of Genetic Factor and Geographical Location on Allicin Content of Garlic (Allium sativum) Germplasm from Egypt and China. Mostafa, Hassan H. A.,Wang Haiping,Liu Xinyan,Li Xixiang,Mostafa, Hassan H. A.. 2015

[11]Large-scale development of expressed sequence tag-derived simple sequence repeat markers by deep transcriptome sequencing in garlic (Allium sativum L.). Liu, Touming.

[12]Multiresidue analysis of 213 pesticides in leek and garlic using QuEChERS-based method and gas chromatography-triple quadrupole mass spectrometry. He, Zeying,Chen, Shanshan,Wang, Lu,Peng, Yi,Luo, Ming,Liu, Xiaowei,Chen, Shanshan,Wang, Wenwen.

[13]Germplasm, production and strategies of garlic and onion in China. Du, WF,Wang, XH. 1997

[14]Yield and economic benefits of late planted short-season cotton versus full-season cotton relayed with garlic. Lu, Hequan,Dai, Jianlong,Li, Weijiang,Tang, Wei,Zhang, Dongmei,Eneji, A. Egrinya,Dong, Hezhong.

[15]Molecularly imprinted polymer solid phase extraction coupled with gas chromatography-mass spectrometry for the determination of trace clenbuterol hydrochloric in animal urine. Wang Pei-Long,Fan Li,Song Rong,Gao Sheng,Su Xiao-Ou,Yang Shu-Ming. 2007

[16]Analysis of volatile oil constituents in pinecone of Pinus koraiensis by gas chromatography-mass spectrometry. Su Xiaoyu,Wang Jing,Yang Xin,Cao Weiqiang. 2006

[17]Evaluation of pesticide residues in fruits and vegetables from Xiamen, China. Chen, Chen,Qian, Yongzhong,Li, Yun,Chen, Qiong,Li, Chuanyong,Tao, Chuanjiang. 2011

[18]Aroma Characterization of 'Flavor No. 3' Melon Using Headspace-Solid Phase Microextraction Combined with Gas Chromatography-Mass Spectrometry. Tang, Mi,Bie, Zhilong,Wu, Mingzhu,Yi, Hongping,Feng, Jiongxin. 2010

[19]Simultaneous Detection of Nine Kinds of Estrogens in Water by Solid Phase Extraction Coupled with Gas Chromatography-Mass Spectrometry. Liao Tao,Wu Xiao-Cui,Wang Shao-Hua,Xiong Guang-Quan,Geng Sheng-Rong,Li Xin,Zu Xiao-Yan,Wu Xiao-Cui,Hu Xiao-Bo,Xie Song-Guang. 2013

[20]Determination of Pentachloronitrobenzene and Its Metabolites in Ginseng by Matrix Solid-Phase Dispersion and GC-MS-MS. Li, Jing,Dong, Fengshou,Liu, Xingang,Zheng, Yongquan,Yao, Jianren,Zhang, Changpeng.

作者其他论文 更多>>