Headspace solid-phase microextraction-gas chromatography-mass spectrometry analysis of the volatile components of longan (Dimocarpus longan Lour.)

文献类型： 外文期刊

第一作者： Zhang, Yi

作者： Zhang, Yi;Gao, Bei;Zhang, Mingwei;Zhang, Yi;Gao, Bei;Zhang, Mingwei;Xu, Yujuan;Shi, John

作者机构：

关键词： Longan;HS-SPME;GC-MS;Volatile components;Optimization;Central composite design

期刊名称：EUROPEAN FOOD RESEARCH AND TECHNOLOGY （ 影响因子：2.998； 五年影响因子：3.005 ）

ISSN： 1438-2377

年卷期： 2009 年 229 卷 3 期

页码：

收录情况： SCI

摘要： Headspace solid-phase microextraction has been applied to the analysis of volatile components in longan (Dimocarpus longan Lour.). Silica fiber coated with divinylbenzene-carboxen-polydimethylsiloxane (DVB-CAR-PDMS) was found to be more efficient for extracting volatile compounds than other fibers such as those coated with polydimethylsiloxane, polyacrylate, and carboxen-polydimethylsiloxane. The SPME headspace volatiles were collected using a DVB-CAR-PDMS fiber. The extraction conditions were optimized using a response surface experimental design to analyze the effect of three factors: extraction temperature, equilibrium time and extraction time. The best response was obtained when the extraction temperature was around 50 A degrees C, equilibrium time near 15 min and extraction time close to 25 min. The volatile extracts were analyzed using gas chromatograph/mass spectrometry system. Sixty-two different volatile compounds from the headspace of longan were identified. The linearity was good in the considered concentration ranges (R (2) a parts per thousand yen 0.965). Average recoveries ranged from 78.6 to 108.3% and showed good accuracy. The precision of the present method was found to be good (RSD < 13.59%). Therefore, this method can be applied to determine the quality of the longan or other volatile components as an alternative to full-scale headspace analysis.

分类号：

  • 相关文献

[1]Analysis of Peanut Using Near-Infrared Spectroscopy and Gas Chromatography-Mass Spectrometry: Correlation of Chemical Components and Volatile Compounds. Lin, Mao,Long, Mingxiu,Zheng, Jiong,Kan, Jianquan,Lin, Mao,Long, Mingxiu,Li, Guolin,Chen, Xi,Lin, Mao,Li, Chao.

[2]GC-MS Analysis of Volatile Components in Chinese Wild Strawberry (F. nilgerrensis Schlecht.). Zhao, M. Z.,Wang, J.,Wang, Z. W.,Qian, Y. M.,Wu, W. M..

[3]A novel Ganoderma lucidum G0119 fermentation strategy for enhanced triterpenes production by statistical process optimization and addition of oleic acid. Feng, Jie,Zhang, Jing-Song,Feng, Na,Yan, Meng-Qiu,Yang, Yan,Jia, Wei,Lin, Chi-Chung,Feng, Jie,Zhang, Jing-Song,Feng, Na,Yan, Meng-Qiu,Yang, Yan,Jia, Wei,Lin, Chi-Chung,Feng, Jie,Zhang, Jing-Song,Feng, Na,Yan, Meng-Qiu,Yang, Yan,Jia, Wei,Lin, Chi-Chung.

[4]Characterization of Fatty Acid, Amino Acid and Volatile Compound Compositions and Bioactive Components of Seven Coffee (Coffea robusta) Cultivars Grown in Hainan Province, China. Dong, Wenjiang,Tan, Lehe,Zhao, Jianping,Hu, Rongsuo,Lu, Minquan,Dong, Wenjiang,Tan, Lehe,Zhao, Jianping,Hu, Rongsuo,Lu, Minquan.

[5]The impact of processing on the profile of volatile compounds in sesame oil. Dong Xu-Yan,Li Ping-Ping,Wei Fang,Jiang Mu-lan,Zhao Ying-Zhong,Li Guang-Ming,Chen Hong,Dong Xu-Yan,Zhao Yuan-Di.

[6]Aroma formation in Dianhong black tea: Effects of baking. Qiu, Xueli,Wang, Jianxin,Yu, Xiaofen,Lv, Shidong,Wu, Yuanshuang,Wang, Chen,Gao, Xuemei,Li, Jiangbing,Zhang, Wenrui,Zhao, Peng,Meng, Qingxiong. 2017

[7]Odor Properties and Volatile Compounds Analysis of Torreya grandis Aril Extracts. Niu, Liying,Bao, Jianfeng,Zhang, Ying,Niu, Liying,Zhao, Lei.

[8]Response surface methodology for the enantioseparation of dinotefuran and its chiral metabolite in bee products and environmental samples by supercritical fluid chromatography/tandem mass spectrometry. Dong, Fengshou,Li, Shasha,Xu, Jun,Liu, Xingang,Zheng, Yongquan,Zheng, Zuntao,Xu, Yongwei.

[9]Optimization of ultrasound-assisted magnetic retrieval-linked ionic liquid dispersive liquid-liquid microextraction for the determination of cadmium and lead in water samples by graphite furnace atomic absorption spectrometry. Wang, Xie,Liu, Haitao,Lin, Chaowen,Pang, Liangyu,Yang, Junwei,Zeng, Qingbin.

[10]Enhancement of botrallin and TMC-264 production in liquid culture of endophytic fungus Hyalodendriella sp Ponipodef12 after treatments with metal ions. Luo, Haiyu,Xu, Dan,Xie, Rushan,Zhang, Xuping,Wang, Jian,Dong, Xuejiao,Lai, Daowan,Zhou, Ligang,Liu, Yang. 2016

[11]Influences of dietary lipid and temperature on growth, fat deposition and lipoprotein lipase expression in darkbarbel catfish (Pelteobagrus vachellii). Qiang, Jun,He, Jie,Li, Hong-Xia,Xu, Pao,Sun, Yi-Lan,Qiang, Jun,Tao, Yi-Fan,Bao, Jin-Wen,Shi, Wen-bo,Xu, Pao. 2017

[12]Influences of Grafting on Aromatic Compounds in Muskmelon by Solid Phase Microextraction with GC-MS. Xiao, Shouhua,Wang, Chongqi,Dong, Yumei,Jiao, Zigao,Zhao, Shancang. 2010

[13]Effects of Exogenous Ethylene Treatments on the Major Volatile Flavor Compounds of Peach Fruit in CA Storage. Wang, Guixi,Liang, Lisong,Hu, Huali,Li, Pengxia. 2008

[14]Analysis of the variation in scent components of Hosta flowers by HS-SPME and GC-MS. Liu, Qian,Sun, Guofeng,Lin, Qinwen,Zhang, Jinzheng,Li, Xiaodong,Liu, Qian,Sun, Guofeng,Lin, Qinwen,Zhang, Jinzheng,Li, Xiaodong,Liu, Qian,Wang, Su.

[15]Enantiomeric and quantitative analysis of volatile terpenoids in different teas (Camellia sinensis). Zhu, Yin,Shao, Chen-Yang,Lv, Hai-Peng,Zhang, Yue,Dai, Wei-Dong,Guo, Li,Tan, Jun-Feng,Peng, Qun-Hua,Lin, Zhi,Shao, Chen-Yang.

[16]Aroma characterisation of Pu-erh tea using headspace-solid phase microextraction combined with GC/MS and GC-olfactometry. Lv, Hai-Peng,Lin, Zhi,Wang, Li,Tan, Jun-Feng,Guo, Li,Zhong, Qiu-Sheng.

[17]Enantiomeric analysis of linalool in teas using headspace solid-phase microextraction with chiral gas chromatography. Yang, Ting,Zhu, Yin,Shao, Chen-Yang,Zhang, Yue,Shi, Jiang,Lv, Hai-Peng,Lin, Zhi,Yang, Ting,Shao, Chen-Yang,Shi, Jiang.

[18]Comparison of Different Extraction Methods in the Analysis of Volatile Compounds in Pomegranate Juice. Yi, Zhiying,Feng, Tao,Li, Mingming,Liu, Tao,Yi, Zhiying,Zhuang, Haining,Ye, Ran.

[19]Burst of reactive oxygen species in pedicel-mediated fruit abscission after carbohydrate supply was cut off in longan (Dimocarpus longan). Yang, Ziqin,Zhong, Xiumei,Wang, Huicong,Li, Jianguo,Huang, Xuming,Yang, Ziqin,Zhong, Xiumei,Fan, Yan. 2015

[20]Recent Advances in Postharvest Research on Longan Fruit. Han, D. M.,Li, J. G.,Pan, X. W.,Li, R.,Guo, D. L.,Han, D. M.,Li, J. G.,Pan, X. W.,Li, R.,Guo, D. L.,Wu, Z. X.,Shuai, L.,Wu, Z. X.. 2014

作者其他论文 更多>>

微信小程序