Determination of Deoxynivalenol-3-Glucoside in Cereals by Hydrophilic Interaction Chromatography with Ultraviolet Detection
文献类型: 外文期刊
第一作者: Geng, Zhiming
作者: Geng, Zhiming;Wang, Daoying;Liu, Fang;Zhu, Yongzhi;Zhang, Muhan;Yang, Dan;Zhou, Miaoping;Zhang, Pingping
作者机构:
关键词: Deoxynivalenol-3-glucoside;Cereal;Hydrophilic interaction chromatography;Ultraviolet detection
期刊名称:FOOD ANALYTICAL METHODS ( 影响因子:3.366; 五年影响因子:3.07 )
ISSN: 1936-9751
年卷期: 2014 年 7 卷 5 期
页码:
收录情况: SCI
摘要: A new hydrophilic interaction liquid chromatography (HILIC) method was developed for the determination of deoxynivalenol-3-glucoside (D3G) in cereals. D3G was extracted with water and cleaned with an immunoaffinity (IA) column, followed by chromatographic separation on a Syncronis HILIC column with acetonitrile-water (90:10, v/v) as the mobile phase, and detected at 220 nm by UV detection. The calibration curve was found to be linear in the range of 0.1-2.0 mu g/ml. Limit of detection and limit of quantification were 8 and 25 mu g/kg, respectively. The method was applied to the determination of D3G in 14 cereal samples, which were analyzed as well as by LC-MS/MS. The results indicate that the method can be considered as an alternative to LC-MS/MS and could be adopted by nonprofessional analytical labs.
分类号:
- 相关文献
作者其他论文 更多>>
-
Genomic and Comparative Transcriptomic Analyses Reveal Key Genes Associated with the Biosynthesis Regulation of Okaramine B in Penicillium daleae NBP-49626
作者:Wang, Yueying;Chen, Ling;Fang, Wei;Zeng, Zhen;Wu, Zhaoyuan;Liu, Fang;Liu, Xiaoyan;Gong, Yan;Zhu, Lei;Wang, Kaimei
关键词:Okaramine B; yield improvement; Penicillium daleae; complete genome; transcriptome; novel regulators; tryptophan metabolism
-
Embedded iron and nitrogen co-doped carbon quantum dots within g-C3N4 as an exceptional PMS photocatalytic activator for sulfamethoxazole degradation: The key role of Fe-N bridge
作者:Zhang, Pingping;Cao, Xiao;Gu, Lin;Yu, Haixiang;Liu, Yifan;Liu, Xinyue;Gao, Yutao;Zhang, Hanlin;Wu, Feiyan;Zhang, Hanlin
关键词:Peroxymonosulfate; Photodegradation; Fe3+/Fe2+cycling; Carbon quantum dots; Graphite-phase carbon nitride
-
Potentially texture-modified food for dysphagia: Gelling, rheological, and water fixation properties of rice starch-soybean protein composite gels in various ratios
作者:Ren, Shuanghe;Zhang, Guofang;Wang, Zhuying;Sun, Fuwei;Cheng, Tianfu;Wang, Zhongjiang;Guo, Zengwang;Wang, Daoying;Yang, Hong
关键词:Rice starch; Soybean protein; Composite gels; Gelling properties; Dysphagia
-
Characterization of HIPEs stabilized by soy protein isolate with excellent rheological properties for 3D printing: Bridging the correlation among structure, function and application
作者:Yuan, Meng;Li, Bailiang;Sun, Fuwei;Cheng, Tianfu;Guo, Zengwang;Wang, Zhongjiang;Liu, Jun;Wang, Daoying
关键词:Soy protein isolate; Oxidation; High internal phase emulsions; Oil -water interface; Rheological properties; 3D printing
-
Comparisons of stripe rust response, grain yield and quality between fungicide sprayed and non-sprayed treatments for newly developed wheat lines carrying different genes for adult-plant resistance to stripe rust
作者:Chen, Hao;Zhang, Liangqi;Ding, Chuanguang;Luo, Yuqi;Jia, Guoyun;Feng, Junming;Wang, Yuqi;Si, Binfan;Zhou, Jianian;Li, Xin;Huang, Kebing;Yang, Suizhuang;Zhou, Xinli;Ren, Yong;Chen, Xianming;Chen, Xianming;Zhang, Pingping;Zhang, Pingping
关键词:Adult -plant resistance; Puccinia striiforms f. sp. tritici; Quality; Stripe rust; Wheat; Yield loss
-
Changes in tenderness of beef M. semitendinosus and modification of actomyosin mediated by Fe(III)-protoporphyrin IX, protoporphyrin IX and free iron
作者:Zhang, Muhan;Shi, Miaomiao;Shu, Lizhi;Ma, Jingjing;Bian, Huan;Wang, Daoying;Yang, Jing;Xu, Weimin;Wei, Suhuan;Guo, Ruirui;Zhang, Muhan;Shi, Miaomiao;Shu, Lizhi;Ma, Jingjing;Bian, Huan;Wang, Daoying;Yang, Jing;Xu, Weimin;Wei, Suhuan;Guo, Ruirui;Zhang, Muhan;Shi, Miaomiao;Shu, Lizhi;Ma, Jingjing;Bian, Huan;Wang, Daoying;Yang, Jing;Xu, Weimin;Wei, Suhuan;Guo, Ruirui
关键词:Porphyrin; Hemin; FeCl 3; Tenderness; Actomyosin dissociation
-
Effects of proteases inactivation on textural quality of yellow-feathered chicken meat and the possible mechanism based on myofibrillar protein
作者:Hao, Danni;Tu, Xiaohang;Zhang, Xinxiao;Guo, Shiyu;Sun, Liangge;Li, Jiaolong;Wang, Daoying;Xu, Weimin;Li, Pengpeng;Hao, Danni;Sun, Liangge;Li, Pengpeng;Tu, Xiaohang;Zhang, Xinxiao;Li, Jiaolong;Wang, Daoying;Wang, Daoying
关键词:Texture; Residual activity of protease; Myofibril; Protein structure; Gel