Determination of Fumonisins B-1, B-2 and Their Hydrolysed Metabolites in Bovine Milk by Liquid Chromatography-Tandem Mass Spectrometry

文献类型： 外文期刊

第一作者： Qian Ming-Rong

作者： Qian Ming-Rong;Wu Li-Qin;Zhang Hu;Li Rui;Chen Zhi-Min;Fang Li-Zhen;Liu Fei

作者机构：

关键词： Milk;Fumonisins;Hydrolysed metabolites;Solid phase extraction;High performance liquid chromatography-tandem mass spectrometry

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2012 年 40 卷 5 期

页码：

收录情况： SCI

摘要： MAX column combined with high performance liquid chromatography- tandem mass spectrometry was used to determine fumonisins B-1 (FB1), FB2 and their hydrolysed metabolites in bovine milk. After 10 mL milk was diluted with 10 mL water, it was directly transferred to MAX column for purification. FB1 and FB2 were eluted with methanol and detected with HPLC-MS/MS in negative mode. The hydrolysed metabolites hydrolysed fumonisins B-1 (HFB1) and HFB2 were eluted with methanol containing 1% acetic acid and detected with HPLC-MS/MS in positive mode. The recoveries for four compounds were 76.4%-92.3% at fortification levels of 0.1-5 mu g/L in bovine milk and relative standard deviation was in the range of 5.9%-12.5%. The LOD was 0.03 mu g/L and LOQ was 0.1 mu g/L for FB1, FB2 and their hydrolysed metabolites. This method is simple, sensitive, and repeatabilities with satisfied recoveries.

分类号：

  • 相关文献

[1]Determination of Fumonisin B-1 and Fumonisin B-2 in Formula Feeds for Livestock and Poultry by High Performance Liquid Chromatography-Tandem Mass Spectrometry. Guo Wen-Bo,Yang Jun-Hua,Han Zheng,Chen Hui-Ying,Sun Zhen-Zhen,Zhao Zhi-Hui,Guo Wen-Bo,Chen Hui-Ying,Sun Zhen-Zhen. 2015

[2]Simultaneous Determination of Residual Quaternary Ammonium Compounds in Milk by Solid Phase Extraction-High Performance Liquid Chromatography-Tandem Mass Spectrometry. Wei Rui-Cheng,Li Guo-Feng,Gong Lan,Chen Ming,Wang Ran,Gao Rong,Sun Ting. 2014

[3]Determination of Alkaloids in Honey by Dispersive Solid Phase Extraction and High Performance Liquid Chromatography-Tandem Mass Spectrometry. Guo Wei-Hua,Zhou Jin-Hui,Huang Jing-Ping,Wang Peng,Li Yi. 2014

[4]Colloidal gold-McAb probe-based rapid immunoassay strip for simultaneous detection of fumonisins in maize. Yao, Jingjing,Sun, Yaning,Li, Qingmei,Wang, Fangyu,Teng, Man,Yang, Yanyan,Deng, Ruiguang,Hu, Xiaofei.

[5]Fumonisin detection and analysis of potential fumonisin-producing Fusarium spp. in asparagus (Asparagus officinalis L.) in Zhejiang Province of China. Wang, Jiansheng,Wang, Xiaoping,Zhou, Ying,Wang, Qiaomei,Wang, Jiansheng,Du, Liangcheng.

[6]Fengycin antibiotics isolated from B-FS01 culture inhibit the growth of Fusarium moniliforme Sheldon ATCC 38932. Hu, Liang Bin,Shi, Zhi Qi,Zhang, Ting,Yang, Zhi Min.

[7]Fumonisins B-1 and B-2 in maize harvested in Hebei province, China, during 2011-2013. Li, Renjie,Guo, Congcong,Pang, Minhao,Liu, Yingchao,Li, Renjie,Guo, Congcong,Liu, Yingchao,Dong, Jingao,Zhang, Quanguo. 2015

[8]Simultaneous Determination of 14 Kinds of beta-Agonist Residues in Sheep Saliva by Ultra Performance Liquid Chramatogrephy-Tandem Mass Spectrometry. Li Yang,Su Xiao-Ou,Wang Rui-Guo,Wang Pei-Long,Zhang Wei,Chen Jie. 2013

[9]Determination of Semiamitraz Residue in Fruits by Solid Phase Extraction-High Performance Liquid Chromatography. Feng Xiao-Yuan,Yang Yuan,Shi Lei,Zhang Kai-Chun,Wang Dong,Zhang Jia,Feng Xiao-Yuan,Wang Bao-Gang. 2010

[10]Determination of Aflatoxin B-1 and Aflatoxin B-2 in Edible Oil by Using Graphene Oxide-SiO2 as Soild Phase Extraction Coupled with HPLC. Wang Heng-Ling,Yu Li,Li Pei-Wu,Li Min,Zhang Qi,Zhang Wen,Wang Heng-Ling,Yu Li,Li Pei-Wu,Li Min,Zhang Wen,Wang Heng-Ling,Li Pei-Wu,Li Min,Zhang Qi,Yu Li,Li Pei-Wu,Zhang Qi. 2014

[11]Determination of Tetracyclines and Their Epimers in Agricultural Soil Fertilized with Swine Manure by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry. Zheng Wen-li,Zhang Li-fang,Zhang Ke-yu,Wang Xiao-yang,Xue Fei-qun. 2012

[12]Silica/graphene oxide nanocomposites: Potential adsorbents for solid phase extraction of trace aflatoxins in cereal crops coupled with high performance liquid chromatography. Yu, Li,Ma, Fei,Ding, Xiaoxia,Wang, Hengling,Li, Peiwu,Yu, Li,Ma, Fei,Li, Peiwu,Yu, Li,Ma, Fei,Li, Peiwu,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Ma, Fei,Ding, Xiaoxia,Wang, Hengling,Li, Peiwu. 2018

[13]Assessment of primary and secondary amine adsorbents and elution solvents with or without graphitized carbon for the SPE clean-up of food extracts in pesticide residue analysis. He, Yan,Liu, Yan-Hong. 2007

[14]UPLC-ESI-MS-MS Determination of Three beta(2)-Agonists in Pork. Zheng, Hong,Yang, Guo-Sheng,Deng, Li-Gang,Lu, Xiao,Zhao, Shan-Cang,Guo, Chang-Ying,Mao, Jiang-Sheng,Wang, Yu-Tao,Deng, Li-Gang,Lu, Xiao,Zhao, Shan-Cang,Guo, Chang-Ying,Mao, Jiang-Sheng,Wang, Yu-Tao,Yang, Guo-Sheng,Aboul-Enein, Hassan Y.,Aboul-Enein, Hassan Y.. 2010

[15]Separation and Determination of Fatty Acid Mono- and Diesters of Monochloropropane-1,2-diol in Fat-rich Foods. Fu Wu-Sheng,Tang Chang-Dong,Wu Shao-Ming,Hua Juan,Wu Yong-Ning,Fang Qin-Mei,Fu Wu-Sheng,Fu Wu-Sheng,Wu Shao-Ming. 2014

[16]Simultaneous Detection of Nine Kinds of Estrogens in Water by Solid Phase Extraction Coupled with Gas Chromatography-Mass Spectrometry. Liao Tao,Wu Xiao-Cui,Wang Shao-Hua,Xiong Guang-Quan,Geng Sheng-Rong,Li Xin,Zu Xiao-Yan,Wu Xiao-Cui,Hu Xiao-Bo,Xie Song-Guang. 2013

[17]Simultaneous determination of triazine herbicides in rice by high-performance liquid chromatography coupled with high resolution and high mass accuracy hybrid linear ion trap-orbitrap mass spectrometry. Mou, Ren-Xiang,Chen, Ming-Xue,Cao, Zhao-Yun,Zhu, Zhi-Wei.

[18]SPE-LC multi-residue analysis of mebendazole and its metabolites in grass carp and shrimp. Jiang, Chaojun,Hui, Yunhua,Shen, Xiaosheng,Zhang, Xiaoling,Yu, Huijuan,Liu, Huan.

[19]Liquid chromatography quadrupole linear ion trap mass spectrometry for multiclass screening and identification of lipophilic marine biotoxins in bivalve mollusks. Wu, Haiyan,Guo, Mengmeng,Tan, Zhijun,Li, Zhaoxin,Zhai, Yuxiu,Wu, Haiyan,Guo, Mengmeng,Tan, Zhijun,Li, Zhaoxin,Zhai, Yuxiu,Wu, Haiyan,Guo, Mengmeng,Tan, Zhijun,Li, Zhaoxin,Zhai, Yuxiu,Wu, Haiyan,Guo, Mengmeng,Tan, Zhijun,Li, Zhaoxin,Zhai, Yuxiu,Cheng, Haiyan.

[20]Comparison of milk samples collected from some buffalo breeds and crossbreeds in China. Sun, Qi,Lv, Jia-ping,Liu, Lu,Zhang, Shu-wen,Liang, Xiao,Lu, Jing.

作者其他论文 更多>>

微信小程序