Rapid detection of fumonisin B-1 and B-2 in ground corn samples using smartphone-controlled portable near-infrared spectrometry and chemometrics
文献类型: 外文期刊
第一作者: Shen, Guanghui
作者: Shen, Guanghui;Kang, Xiaocun;Su, Jianshuo;Qiu, Jianbo;Liu, Xin;Xu, Jianhong;Shi, Jianrong;Xu, Jianhong;Shi, Jianrong;Mohamed, Sherif Ramzy
作者机构:
关键词: Corn; Portable near-infrared spectrometer; Fumonisin; Rapid detection
期刊名称:FOOD CHEMISTRY ( 影响因子:9.231; 五年影响因子:8.795 )
ISSN: 0308-8146
年卷期: 2022 年 384 卷
页码:
收录情况: SCI
摘要: A portable near-infrared (NIR) spectrometer coupled with chemometrics for the detection of fumonisin B-1 and B-2 (FBs) in ground corn samples was proposed in the present work. A total of 173 corn samples were collected, and their FB contents were determined by HPLC-MS/MS. Partial least squares (PLS), support vector machine (SVM) and local PLS based on global PLS score (LPLS-S) algorithms were employed to construct quantitative models. The performance of the SVM and LPLS-S was better than that of PLS, and the LPLS-S presented the lowest RMSEP (12.08 mg/kg) and the highest RPD (3.44). Partial least squares-discriminant analysis (PLS-DA) and support vector machine-discriminant analysis (SVM-DA) were used to classify corn samples according to the maximum residue limit (MRL) of FBs, and the discriminant accuracy of both the PLS-DA and SVM-DA algorithms was above 86.0%. Thus, the present study provided a rapid method for monitoring FB contamination in corn samples.
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