Determination of retrorsine in orange peel by Ultra-high-performance liquid chromatography tandem mass
文献类型： 外文期刊
作者： Chen, Wuhai 1 ; Zeng, Shaodong 1 ; Jia, Ning 3 ; Liu, Zuhong 2 ; Qi, Ningli 1 ; Pan, Xiaowei 1 ; Ye, Jianzhi 1 ;
作者机构： 1.Chinese Acad Trop Agr Sci, Agr Prod Proc Res Inst, Zhan Jiang 524001, Guangdong, Peoples R China
2.Yunnan Agr Univ, Coll Trop Crops, Pu Er 665099, Yunnan, Peoples R China
3.Huazhong Agr Univ, Coll Food Sci & Technol, Wuhan 430070, Peoples R China
期刊名称：2020 2ND INTERNATIONAL CONFERENCE ON CIVIL ENGINEERING, ENVIRONMENT RESOURCES AND ENERGY MATERIALS
ISSN： 1755-1307
年卷期： 2021 年 634 卷
页码：
收录情况： SCI
摘要： A method for the determination of retrorsine in orange peel by ultra performance liquid chromatography tandem mass spectrometry (LC-MS/MS) was established. The acetonitrile (containing 0.1% formic acid) was extracted, ionized by electrospray ionization with positive ion mode and determined by multi-reaction monitoring mode. The results showed a good linearity in the range of 0.2-2.0 ng/mL, and the correlation Coefficient R-2 was 0.998453. The average recoveries of the three additive levels were more than 70% and the RSD was 0.19%-1.57%. The method was sensitive and rapid, and could be used for the determination of retrorsine in orange peel by ultra performance liquid chromatography tandem mass spectrometry.
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