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Preparation and Characterization of FeCo Alloy Nanoparticles

文献类型: 外文期刊

作者: Wang, Fengping 1 ; Xue, Xinghua 1 ; Wang, Guizhen 2 ; Cai, Jingyao 2 ; Fu, Xin 2 ;

作者机构: 1.Chinese Acad Trop Agr Sci, Rubber Res Inst, Danzhou 571737, Peoples R China

2.Hainan Univ, Coll Mat & Chem Engn, Haikou 570228, Peoples R China

关键词: FeCo nanoparticles;preparation;structure;magnetic property

期刊名称:INTEGRATED FERROELECTRICS ( 影响因子:0.836; 五年影响因子:0.787 )

ISSN: 1058-4587

年卷期: 2011 年 128 卷

页码:

收录情况: SCI

摘要: FeCo alloy nanoparticles were synthesized by a new reduction process in liquid phase with sodium borohydride and L-ascorbic acid as reductant, and cetyltrimethylammonium bromide as surfactant. The structure and magnetic properties of the samples were investigated by laser particle size analyzer, X-ray powder diffraction, transmission electron microscopy, selected-area electron diffraction and vibrating sample magnetometer. The nanoparticles obtained are nearly spherical and have a body-centred cubic structure. The average size of the particles is 75 nm. The saturation magnetization and coercivity are 56.6 emu/g and 20 Oe, respectively. The FeCo nanoparticles do not indicate an ideal superparamagnetic behaviour with no hysteresis at room temperature.

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