Magnetic polymer particles as a highly efficient and facile cleanup adsorbent for multi-pesticide residues analysis in aquatic products
文献类型： 外文期刊
作者： Liu, Zhenzhen 1 ; Zhao, Huiyu 1 ; Wang, Jiao 1 ; Wang, Zhiwei 1 ; Di, Shanshan 1 ; Xu, Hao 1 ; Wang, Qiang 1 ; Wang, Xinhong 2 ; Wang, Xinquan 1 ; Qi, Peipei 1 ;
作者机构： 1.Zhejiang Acad Agr Sci, Inst Agroprod Safety & Nutr, State Key Lab Managing Biot & Chem Threats Qual &, Hangzhou 310021, Peoples R China
2.Xiamen Univ, Coll Environm & Ecol, State Key Lab Marine Environm Sci, Xiamen 361005, Peoples R China
3.Agr Minist Key Lab Pesticide Residue Detect, Hangzhou 310021, Peoples R China
4.Key Lab Detect Pesticide Residues & Control Zhejia, Hangzhou 310021, Peoples R China
5.Xiangan South Rd, Xiamen 361102, Peoples R China
6.198 Shiqiao Rd, Hangzhou 310021, Peoples R China
关键词： Magnetic particles; Multi -pesticide residues; Aquatic products; Liquid chromatography -tandem mass spectrometry
期刊名称：ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY （ 影响因子：7.129； 五年影响因子：7.284 ）
ISSN： 0147-6513
年卷期： 2022 年 241 卷
页码：
收录情况： SCI
摘要： A novel and efficient sample pretreatment procedure using magnetic particles was exploited for the determi-nation of multi-pesticide residues in aquatic products. The magnetic adsorbent was prepared using divinyl benzene and N-vinyl pyrrolidone as functional monomers modified on the Fe3O4 @SiO2. The obtained magnetic adsorbent, octadecylsilane sorbents, and graphitized carbon black were employed as effective adsorbents to remove matrix interferences in aquatic products, and their dosages were optimized. Satisfactory levels of ac-curacy and precision were procured under optimum conditions. The method limits of quantification ranged from 0.1 to 2.0 mu g/kg. The analytical accuracy of the developed method for the analysis of multi-pesticide residues in freshwater and seafood products was validated. It was found to be suitable for the analysis of multi-pesticide residues in different types of aquatic products. Additionally, the method was successfully applied for the anal-ysis of pesticide residues in fish samples obtained from aquaculture plants located in Zhejiang Province, China. The detected concentrations of pesticides ranged from 0.14 to 0.95 mu g/kg. In general, this method shows promising application prospects for the rapid determination of multi-pesticide residues in aquatic products.
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