Simultaneous analysis of PAEs in edible oil and dietary exposure assessment in Hubei

文献类型: 外文期刊

第一作者: Wei, Hailian

作者: Wei, Hailian;Yang, Xianglong;Cheng, Ling;Zhang, Qi;Mao, Jin;Li, Peiwu;Yang, Xianglong;Cheng, Ling;Zhang, Qi;Mao, Jin;Li, Peiwu

作者机构:

关键词: Accurate quantification; Efficient extraction; Gas chromatography-mass spectrometry; Risk assessment; Response surface methodology

期刊名称:FOOD CHEMISTRY ( 影响因子:9.8; 五年影响因子:9.7 )

ISSN: 0308-8146

年卷期: 2025 年 468 卷

页码:

收录情况: SCI

摘要: Phthalic acid esters (PAEs), widely used in food processing, pose significant risks to food safety and human health. A rapid and accurate method to simultaneously detect 18 PAEs in edible oil was developed and applied to evaluate daily exposures in Hubei. By using ultrasound-assisted extraction and GC-MS with deuterated isotopes, we improved extraction efficiency and detection accuracy. The method exhibited excellent linearity and low limits of quantification, with average recoveries ranging from 84.32 % to 115.80 % and relative standard deviations between 2.08% and 12.82%. Among 30 commercial edible oils analyzed, higher average levels of DBP, DEHP, and DINP were found at 0.207, 1.767, and 0.600 mg/kg, respectively. Dietary exposure assessment indicated that daily intakes were below health guideline values, but DEHP posed a relatively higher health risk. These findings provide a simple method and reference for assessing PAEs exposure and health risk in edible oil.

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