Preparation and characterization of highly dispersed nanocrystalline rutile powders

文献类型： 外文期刊

第一作者： Liu, Zhao-Tie

作者： Liu, Zhao-Tie;Yao, Shushan;Sun, Ping;Song, Liping;Lu, Jian;Xiong, Heping;Peng, Yuande;Tang, Shouwei

作者机构：

关键词： nano-titania;rutile;dispersibility;preparation;microstructure

期刊名称：MATERIALS LETTERS （ 影响因子：3.423； 五年影响因子：3.003 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A highly dispersed nanocrystalline rutile powder (NRP) having ultrafme and narrow-distributed diameters was successfully prepared via an improved conventional liquid one-step method by introducing dioctyl sulfosuccinate sodium salt (AOT) surfactant in the peptization reaction anaphase. The average grain size of the product is 10-20 nm. The effects of the titanium tetrabutoxide (Ti(OBu)_4) to ethanol volumetric ratio, the precipitation temperature, the peptization temperature and the presence of dioctyl sulfosuccinate sodium salt (AOT) on the preparation of NRP were studied. A new procedure for synthesizing NRP is proposed, and the optimum conditions for preparing NRP were obtained. The TEM, XRD, SEM and FT-IR results were also investigated in this work.

分类号： TB3

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