2-D RP/RPLC method to separate components in Fructus schisandrae chinensis

文献类型： 外文期刊

第一作者： Jin, Gaowa

作者： Jin, Gaowa;Feng, Jiatao;Xue, Xingya;Zhang, Feifang;Liang, Xinmiao;Jin, Gaowa;Dai, Yuntao;Qin, Xuemei;Zhang, Feifang;Liang, Xinmiao

作者机构：

关键词： beta-CD column;Fructus schisandrae chinensis;Traditional Chinese medicine;2-D RP/RPLC

期刊名称：JOURNAL OF SEPARATION SCIENCE （ 影响因子：3.645； 五年影响因子：2.943 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： An off-line 2-D RP/RPLC method was developed to separate components in extracts of Fructus schisandrae chinensis, which is a traditional Chinese medicine. In this method, Click beta-CD stationary phase was proposed for constructing 2-D RP/RPLC system combined with C18 column. beta-CD column showed great potential to separate compounds in traditional Chinese medicines under RP mode. Collected fractions from Click beta-CD column used in first dimension were resolved into many additional components, indicating that the 2-D LC system based on Click beta-CD and C18 phases is orthogonal. The mobile phase was same on both columns. This 2-D LC method facilitates us not only to separate components that cannot be resolved by unidimensional chromatography, but also to achieve much more efficient detection of minor sample components.

分类号： O6

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