A simple fluorescence pyrocatechol-polyethyleneimine detection method for 3-MCPD

文献类型: 外文期刊

第一作者: Xu, Ting

作者: Xu, Ting;Fu, Qing;Qingru, Zeng;Wang, Zhaojie;Liu, Xin;Xiao, Shensheng;Gong, Zhiyong;Fang, Min;Liu, Xin;Xiao, Shensheng;Gong, Zhiyong;Fang, Min;Jiang, Xiaoming;Lu, Yuepeng;Wu, Yongning

作者机构:

期刊名称:ANALYTICAL METHODS ( 影响因子:3.1; 五年影响因子:3.0 )

ISSN: 1759-9660

年卷期: 2024 年 16 卷 2 期

页码:

收录情况: SCI

摘要: A rapid fluorescence detection method was established for 3-monochloropropane-1,2-diol (3-MCPD). The detection system works based on the fluorescence quenching of pyrocatechol-polyethyleneimine (PCh-PEI) polymer by 3-MCPD. The fluorescence quenching ability of 3-MCPD for PCh-PEI polymer was measured at different pH and temperatures. Indeed, in the presence of 3-MCPD, the fluorescence intensity of PCh-PEI polymer solution was quenched best at 100 degrees C and pH 8.5. Also, the effect of different concentrations of 3-MCPD on the optical properties of the PCh-PEI polymer was examined. Under optimal experimental conditions, fluorescence detection was linear in a range of 0.08-2.0 mg per L 3-MCPD, with a calculated detection limit of 0.06 mg L-1 and a correlation coefficient of 0.9974. Concisely, the reported method has good sensitivity and can be used for the rapid detection of 3-MCPD contamination in food products. A rapid fluorescence detection method was established for 3-monochloropropane-1,2-diol (3-MCPD).

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