Determination of 6 biogenic amines in food using high-performance liquid chromatography-tandem mass spectrometry without derivatization
文献类型： 外文期刊
第一作者： Zhang, Xuan
作者： Zhang, Xuan;Hui, Yunhua;Jiang, Mei;Cai, Youqiong;Huang, Dongmei;Yang, Guangxin;Kong, Cong
作者机构：
关键词： Biogenic amines; Histamine; HILIC; High-performance liquid chromatography-tandem mass spectrometry
期刊名称：JOURNAL OF CHROMATOGRAPHY A （ 影响因子：4.759； 五年影响因子：4.302 ）
ISSN： 0021-9673
年卷期： 2021 年 1653 卷
页码：
收录情况： SCI
摘要： A rapid and simple method for the determination of 6 biogenic amines (BAs) in food was established on HPLC-MS /MS without derivatization. Samples were extracted with 5% perchloric acid and cleaned with n-hexane for lipid removal. The analytes were separated on Waters XBridge (R) HILIC (150 mm x 2.1 mm, 3.5 mu m) and analyzed with multiple-reaction monitoring (MRM) mode after positive electrospray ionization on HPLC-MS/MS. Good linearity with high correlation coefficient was obtained between 1010 0 0 mu g/L for cadaverine (CAD), putrescine (PUT), tyramine (TYR) and 2-phenylethylamine (2-PHE) and between 1-100 mu g/L for histamine (HIS) and tryptamine (TRY), with the detection limits of the method ranging from 0.1 mg/kg for HIS and TRY, and 1.0 mg/kg for CAD, PUT, TYR and 2-PHE, which are under the residue limit of Chinese regulation. Spiking experiments demonstrated good recoveries between 70.2114.6%, with relative standard deviations (RSDs) between 0.44-13.01%. This method was validated for BAs determination in liquor, fermented meat products, vegetable products, soybean products, dairy products, seafood and its derived products. These results promise high feasibility for BAs monitoring in various food with easy-to-operate and fast sample preparation process, stable analysis on HPLC-MS/MS without derivatization. (c) 2021 Elsevier B.V. All rights reserved.
分类号：
- 相关文献
作者其他论文 更多>>
-
The impact of climate policy uncertainty on urban climate risk: Evidence from 274 cities in China
作者：Zhang, Hanying;Liu, Jing;Guo, Qing;Zhang, Xuan;Hu, Xiangdong
关键词：Climate policy uncertainty; Urban climate risk; Industrial structure; Household deposit balance; Insurance cost
-
Methyl jasmonate attenuates chilling injury of prune fruit by maintaining ROS homeostasis and regulating GABA metabolism and energy status
作者：Zhao, Yating;Wu, Yingjie;Zhang, Xuan;Zhu, Xuan;Li, Xuewen;Wu, Wenxin;Hou, Yuanyuan;Chen, Jianye;Cui, Kuanbo
关键词：Methyl jasmonate; Prune fruit; Chilling injury; ROS homeostasis; GABA; Energy status
-
Eco-friendly chitosan microspheres as a novel one-step sorbent for the rapid purification and determination of pesticides and veterinary drug multi-residues in aquatic products with HPLC-MS/MS
作者：Zhou, Ruidong;Wen, Yupeng;Huo, Wendi;Liu, Huan;Zhang, Chaoying;Mu, Yingchun;Li, Jincheng;Zhou, Ruidong;Wen, Yupeng;Huo, Wendi;Liu, Huan;Zhang, Chaoying;Mu, Yingchun;Li, Jincheng;Kong, Cong;Yang, Guangxin;Huang, Dongmei
关键词：Chitosan microspheres; Sorbent; Pesticides and veterinary drugs; QuEChERS; Aquatic products
-
Acute Toxicity, Bioaccumulation and Elimination Rate of Deltamethrin and Cypermethrin in Crucian Carp (Carassius auratus)
作者：Jiang, Zhongquan;Ji, Yunyun;Xie, Xinyi;Yang, Guangxin;Kong, Cong;Shen, Xiaosheng;Jiang, Zhongquan;Xing, Ruikai
关键词：deltamethrin; cypermethrin; acute toxicity; bioaccumulation; elimination; Carassius auratus
-
Establishment of an efficient regeneration system for Lycium barbarum
作者：Zhang, Xuan;Ma, Ximei;Yang, Gaier;Li, Xiang;Zhang, Xuan;Ma, Ximei;Yang, Gaier;Li, Xiang;Yin, Xiao;Yao, Wenkong;Tigabu, Mulualem;Zhang, Bo;Duan, Linyuan
关键词：Lycium barbarum; Regeneration system; Tissue culture; Adventitious root; Adventitious buds
-
Comprehensive Insights of Biochemical and Sensory Characterization in Takifugu obscurus by Environmental Modulation
作者：Li, Siman;Huang, Xuanyun;Fang, Changling;Shi, Yongfu;Lou, Xiaoyi;Huang, Dongmei;Tang, Yunyu
关键词：
Takifugu obscurus ; pufferfish; salinity; season; fasting; sensory; nutrition -
Engineering the key domains of starch synthases and branching enzyme to balance the amylose increase and yield loss in maize kernels
作者：Wang, Zhengqi;Hu, Shuting;Zhang, Xuan;Ge, Xingyu;Xu, Sixuan;Li, Jiansheng;Yang, Xiaohong;Wang, Zhengqi;Hu, Shuting;Zhang, Xuan;Ge, Xingyu;Xu, Sixuan;Li, Jiansheng;Yang, Xiaohong;Wang, Zhengqi;Xu, Sixuan;Li, Jiansheng;Yang, Xiaohong;Zhuang, Junhong;Zhao, Xiaoming;Wang, Xiqing;Li, Jiansheng;Yang, Xiaohong;Tang, Huaijun;Yang, Xiaohong
关键词：Maize; Gene editing; SSIIa; SBEIIb; High-amylose starch
