Determination of retrorsine in orange peel by Ultra-high-performance liquid chromatography tandem mass

文献类型： 外文期刊

第一作者： Chen, Wuhai

作者： Chen, Wuhai;Zeng, Shaodong;Qi, Ningli;Pan, Xiaowei;Ye, Jianzhi;Liu, Zuhong;Jia, Ning

作者机构：

期刊名称：2020 2ND INTERNATIONAL CONFERENCE ON CIVIL ENGINEERING, ENVIRONMENT RESOURCES AND ENERGY MATERIALS

ISSN： 1755-1307

年卷期： 2021 年 634 卷

页码：

收录情况： SCI

摘要： A method for the determination of retrorsine in orange peel by ultra performance liquid chromatography tandem mass spectrometry (LC-MS/MS) was established. The acetonitrile (containing 0.1% formic acid) was extracted, ionized by electrospray ionization with positive ion mode and determined by multi-reaction monitoring mode. The results showed a good linearity in the range of 0.2-2.0 ng/mL, and the correlation Coefficient R-2 was 0.998453. The average recoveries of the three additive levels were more than 70% and the RSD was 0.19%-1.57%. The method was sensitive and rapid, and could be used for the determination of retrorsine in orange peel by ultra performance liquid chromatography tandem mass spectrometry.

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