Rapid determination of trans-resveratrol in vegetable oils using magnetic hydrophilic multi-walled carbon nanotubes as adsorbents followed by liquid chromatography-tandem mass spectrometry

文献类型： 外文期刊

第一作者： Ma, Fei

作者： Ma, Fei;Li, Peiwu;Zhang, Qi;Yu, Li;Zhang, Liangxiao;Ma, Fei;Li, Peiwu;Zhang, Qi;Yu, Li;Zhang, Liangxiao;Ma, Fei;Li, Peiwu;Zhang, Qi;Yu, Li;Zhang, Liangxiao;Ma, Fei;Li, Peiwu;Yu, Li;Zhang, Liangxiao;Li, Peiwu;Zhang, Qi

作者机构：

关键词： trans-Resveratrol;Magnetic multi-walled carbon nanotubes;Edible oils;Liquid chromatography-tandem mass spectrometry

期刊名称：FOOD CHEMISTRY （ 影响因子：7.514； 五年影响因子：7.516 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： In the present work, a rapid and simple procedure was developed and validated for the analysis of trans-resveratrol in vegetable oils based on magnetic hydrophilic multi-walled carbon nanotubes (h-MWCNT-MNPs) combined with liquid chromatography-tandem mass spectrometry (LC-MS/MS). h-MWCNT-MNPs were simply obtained by wrapping amine-functionalized Fe3O4 magnetic nanoparticles into previously oxidized hydrophilic multi-walled carbon nanotubes. The major parameters affecting extraction efficiency were investigated, including the type and volume of desorption solvents, extraction and desorption time, washing solution, and sorbent amount. The limit of detection (LOD) and the limit of quantification (LOQ) were calculated as 0.6 and 2.0 mu g/kg, respectively. The recoveries of trans-resveratrol in oil samples were in the range of 90.0-110.0% with RSDs of less than 17.5%. The results showed that only peanut oil contained trans-resveratrol, ranging from 8 +/- 1 to 103 +/- 12 mu g/kg. The proposed method is reliable and robust, having an excellent potential for the analysis of trans-resveratrol in edible oils. (C) 2015 Elsevier Ltd. All rights reserved.

分类号： TS2`TS201.2

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