Simultaneous quantification of six major triterpenoid saponins in Schefflera kwangsiensis using high-performance liquid chromatography coupled to orbitrap mass spectrometry

文献类型： 外文期刊

第一作者： Zhang, Leilei

作者： Zhang, Leilei;Zhang, Leilei;Wang, Yan;Yu, De-Quan;Wang, Yan;Yu, De-Quan;Wang, Yan

作者机构：

关键词： Schefflera kwangsiensis;triterpenoid saponins;quantitative analysis;HPLC-ESI-MS

期刊名称：NATURAL PRODUCT RESEARCH （ 影响因子：2.861； 五年影响因子：2.572 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A simple and accurate analytical method was developed for simultaneous and quantitative analysis of six triterpenoid saponins in Schefflera kwangsiensis via high-performance liquid chromatography (HPLC) with mass spectrometry (MS) in this study. Separation was performed on a Thermo hypersil GOLD C_(18) column (150 mm X2.1mm, 5 mum). A mobile phase consisting of methanol/acetonitrile/8 mM ammonium acetate in water was used with a flow rate of 0.3 mL/min. The analytes were detected by MS with the electrospray ionisation (ESI) source combined with negative monitoring and full scan mode, and were analysed by extracted ion chromatography. This established HPLC-ESI-MS analysis demonstrated good linearity, sensitivity, stability, precision, accuracy and recovery. Therefore, this analytical method has great potential to be a novel tool to qualify S. kwangsiensis.

分类号： R9

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