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MANNICH-TYPE REACTION FOR SYNTHESIS OF 3-METHYL-4-NITROIMINO-TETRAHYDRO-1,3,5-OXADIAZINE

文献类型：外文期刊

第一作者： She, Dong-Mei

作者： She, Dong-Mei;Zhao, Jian;Lin, De-Jie;Huang, Qi-Liang;Li, Feng-Min

作者机构：

关键词： Formaldehyde;Mannich reaction;3-methyl-4-nitroimino-tetrahydro-1,3,5-oxadiazine;N-(1,5-dimethyl-1,3,5-triazinan-2-ylidene)nitramide;N-(5-ethyl-1-methyl-1,3,5-triazinan-2-ylidene)nitramide;N-methyl-N '-nitroguanidine

期刊名称：SYNTHETIC COMMUNICATIONS （影响因子：2.007；五年影响因子：1.717 ）

ISSN： 0039-7911

年卷期： 2012 年 42 卷 13 期

页码：

收录情况： SCI

摘要： The reaction of N-methyl-N'-nitroguanidine with 3-methyl-4-nitroiminotetrahydro-1,3,5-oxadiazine is a Mannich-type reaction. The reaction was catalyzed by several organic and inorganic bases at different reaction times and temperatures. Three inorganic base catalysts [potassium carbonate (K2CO3), sodium hydrogen carbonate (NaHCO3), and sodium hydroxide (NaOH)] and several organic bases (methylamine, ethamine, iso-propylamine, and n-butylamine) have been studied. The results showed that both the inorganic and organic base catalysts can be used as catalysts, with the organic bases performing better. N-Methyl-N'-nitroguanidine reacts to give the title compound 2 and is catalyzed by both acids and bases. The intensity of inorganic base catalysts, reaction temperature, and reaction time had significant effects on the products.

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