Application of on-line dialysis in the determination of nitrite and nitrate in vegetables by ion chromatography

文献类型： 外文期刊

第一作者： Xu Xia

作者： Xu Xia;Ying Xing-Hua;Duan Bin-Wu;Chen Neng

作者机构：

关键词： dialysis;ion chromatography;vegetables;nitrite;nitrate

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2007 年 35 卷 11 期

页码：

收录情况： SCI

摘要： An on-line dialysis coupling with ion chromatographic method for the simultaneous determination of nitrite and nitrate in vegetables using suppressed conductivity detection was reported. The nitrite and nitrate were extracted from the vegetable by mixing and diluting the samples with boiled water. The water-soluble giant molecule, impurity and pigment etc. were removed by on-line dialysis with dialysis cellulose acetate membrane of pore size 0. 20 mu m. A standard or sample containing the anions was separated on an anion-exchange column (250 mm x 4 mm) with 1.8 mmol/L Na2CO3 + 1.7 mmol/L NaHCO3 as eluent and was detected by suppressed conductivity detector. Parameters such as linearity, limit of detection, precision and accuracy of the method were investigated. The relative standard deviation for the proposed method was lower than 10% and considering a sample of 20. 0 g ( n = 6), the detection limit of the method was 0. 075 mg/kg and 0. 105 rng/kg of nitrite and nitrate, respectively. The recoveries of nitrite and nitrate in vegetable matrices were 80. 6% - 98. 7% and 90. 5% - 114%, respectively. The proposed method was compared with a reference method official AOAC reference method for the determination of nitrite and nitrate in foodstuffs). These results demonstrated that the proposed method is simple, sensitive and reliable for the determination of nitrite and nitrate in vegetables, despite the presence of the particularly complex matrix.

分类号：

  • 相关文献

[1]Denitrification-dependent anammox activity in a permanently flooded fallow ravine paddy field. Zhou, Sheng,Borjigin, Sodbilig,Riya, Shohei,Hosomi, Masaaki,Borjigin, Sodbilig.

[2]The relationship between anammox and denitrification in the sediment of an inland river. Zhou, Sheng,Zhou, Sheng,Borjigin, Sodbilig,Riya, Shohei,Terada, Akihiko,Hosomi, Masaaki.

[3]Evaluation of nitrification inhibitor 3,4-dimethyl pyrazole phosphate on nitrogen leaching in undisturbed soil columns. Yu, Qiaogang,Chen, Yingxu,Ye, Xuezhu,Zhang, Qiuling,Zhang, Zhijian,Tian, Ping.

[4]Changes in the soil environment from excessive application of fertilizers and manures to two contrasting intensive cropping systems on the North China Plain. Ju, X. T.,Kou, C. L.,Christie, P.,Dou, Z. X.,Zhang, F. S..

[5]Investigations on Nitrate Pollution of Soil, Groundwater and Vegetable from Three Typical Farmlands in Beijing Region, China. Du Lian-feng,Zhao Tong-ke,Zhang Cheng-jun,An Zhi-zhuang,Wu Qiong,Liu Bao-cun,Li Peng,Ma Mao-ting. 2011

[6]Effect of nitrogen form and root-zone pH on growth and nitrogen uptake of tea (Camellia sinensis) plants. Ruan, Jianyun,Gerendas, Joska,Hardter, Rolf,Sattelmacher, Burkhard.

[7]Determination of Inosine Monophosphate in Meat Products by Ion Chromatography with Suppressed Conductivity Detection. Zhu Zuo-Yi,Zhang Yu,Wang Jun-Hong,Li Xue,Wang Wei,Zhu Zuo-Yi,Zhang Yu,Wang Wei,Zhu Zuo-Yi,Zhang Yu,Wang Wei. 2015

[8]Determination of Inorganic Cations and Anions in Chitooligosaccharides by Ion Chromatography with Conductivity Detection. Li, Xiuhuan,Zheng, Li,Wu, Miaomiao,Huang, Qiliang,Fan, Li,Zhang, Shanxue. 2017

[9]Determination of soluble sugar profile in rice. Hu, Xianqiao,Fang, Changyun,Lu, Lin,Hu, Zhanqiang,Shao, Yafang,Zhu, Zhiwei,Hu, Xianqiao,Fang, Changyun,Lu, Lin,Hu, Zhanqiang,Shao, Yafang,Zhu, Zhiwei.

[10]DEGRADATION PRODUCTS OF CHINESE SILVERGRASS BY (CO)-C-60 Gamma-RAY IRRADIATION PRETREATMENT. Li, Qingming,Su, Xiaojun,Xiong, Xingyao,Hu, Qiulong,Li, Qingming,Jiang, Yile,Su, Xiaojun,Tan, Xinghe,Yu, Songwen,Xiong, Xingyao. 2015

[11]Determination of Anions and Cations in Biodiesel with On-line Sample Pretreatment Column-switching Ion Chromatography. Huang, Zhongping,Pan, Zaifa,Wang, Lili,Zhao, Xunyan,Zhu, Yan,Zhu, Zuoyi.

[12]Analysis of trace inorganic anions in weak acid salts by single pump cycling-column-switching ion chromatography. Huang, Zhongping,Pan, Zaifa,Wang, Lili,Ni, Chengzhu,Zhu, Yan,Zhu, Zhuyi.

[13]Determination of Free and Total Sulfite in Red Globe Grape by Ion Chromatography. Lin, Jiangli,Zhu, Yajuan,Cheng, Wenhu,Wang, Jinxia,Wang, Jide,Wu, Bin.

[14]Nitrate and Inhibition of Ruminal Methanogenesis: Microbial Ecology, Obstacles, and Opportunities for Lowering Methane Emissions from Ruminant Livestock. Yang, Chengjian,Rooke, John A.,Cabeza, Irene,Wallace, Robert J.. 2016

[15]Promotion of the Growth and Quality of Chinese Cabbage by Application of Biogas Slurry of Water Hyacinth. Xue, Yanfeng,Shi, Zhiqi,Chen, Jian,Yan, Shaohua,Zheng, Jianchu. 2012

[16]Identification and mRNA expression of antioxidant enzyme genes associated with the oxidative stress response in the Wuchang bream (Megalobrama amblycephala Yih) in response to acute nitrite exposure. Sun, Shengming,Ge, Xianping,Zhu, Jian,Xuan, Fujun,Jiang, Xiaojun. 2014

[17]Synthesis of Fluorescent Gold Nanoclusters Directed by Bovine Serum Albumin and Application for Nitrite Detection. Yue, Qiaoli,Sun, Lijun,Shen, Tongfei,Liu, Jifeng,Gu, Xiaohong,Zhang, Shuqiu. 2013

[18]Optimization of nitrite reductase production conditions in Lactobacillus plantarum from salted fish. Wang, Yanan,Wu, Yanyan,Yang, Xianqing,Li, Laihao,Qi, Bo. 2013

[19]Effects of nitrite exposure on haematological parameters, oxidative stress and apoptosis in juvenile turbot (Scophthalmus maximus). Jia, Rui,Huo, Huan-Huan,Jia, Rui,Lei, Ji-Lin,Liu, Bao-Liang,Huang, Bin,Yin, Shu-Ting,Han, Cen.

[20]Molecular cloning, tissue distribution and expression analysis of a manganese superoxide dismutase in blunt snout bream Megalobrama amblycephala. Sun, Shengming,Zhu, Jian,Li, Bing,Ge, Xianping,Jiang, Xiaojun,Ge, Xianping.

作者其他论文 更多>>

微信小程序