Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS

文献类型： 外文期刊

第一作者： Liu, Hongcheng

作者： Liu, Hongcheng;Shao, Jinliang;Lin, Tao;Li, Qiwan

作者机构：

关键词： GC-MS;Ultrasound-assisted matrix solid-phase dispersion;Benzo[a]pyrene;Fried food

期刊名称：CHROMATOGRAPHIA （ 影响因子：2.044； 五年影响因子：1.725 ）

ISSN： 0009-5893

年卷期： 2013 年 76 卷 23-24 期

页码：

收录情况： SCI

摘要： A simple, sensitive and reliable analytical method was developed for the detection of benzo[a]pyrene in fried food using gas chromatography-mass spectrometry with an isotope-labelled internal standard. Samples were directly extracted and purified by the ultrasound-assisted matrix solid-phase dispersion (MSPD) procedure. The simple pretreatment procedures were tested with different absorbents (C18, NH2, Oasis, and SiO2). The optimal ultrasonication-assisted MSPD was achieved by MSPD-SiO2 and sonication for 10 min in an ultrasonic bath. The samples were quantified using benzo[a]pyrene-d(12) as the internal standard. An analysis of the samples spiked with different levels of benzo[a]pyrene showed recoveries ranging from 84.6 to 103.2 %, with an RSD of 3.21-8.32 %, depending on the spiking level. This method was thus shown to be suitable for the detection of benzo[a]pyrene in fried food.

分类号：

  • 相关文献

[1]Biodegradation of pyrene and benzo[a]pyrene in the liquid matrix and soil by a newly identified Raoultella planticola strain. Ping, Lifeng,Yuan, Xiaoli,Ping, Lifeng,Guo, Qian,Chen, Xiaoyang,Zhang, Chunrong,Zhao, Hua. 2017

[2]Isolation and characterization of pyrene and benzo[a]pyrene-degrading Klebsiella pneumonia PL1 and its potential use in bioremediation. Ping, Lifeng,Zhang, Chunrong,Zhang, Changpeng,Zhu, Yahong,He, Hongmei,Wu, Min,Tang, Tao,Li, Zhen,Zhao, Hua,Ping, Lifeng,Zhang, Chunrong,Zhang, Changpeng,Zhu, Yahong,He, Hongmei,Wu, Min,Tang, Tao,Li, Zhen. 2014

[3]Chemical compositions and volatile compounds of Tricholoma matsutake from different geographical areas at different stages of maturity. Li, Xiaolin,Zheng, Linyong,Zhang, Li,Yang, Hua,Li, Wanhua,Huang, Wenli,Zheng, Linyong. 2016

[4]Composition and morphology of cuticular wax in blueberry (Vaccinium spp.) fruits. Chu, Wenjing,Gao, Haiyan,Fang, Xiangjun,Chen, Hangjun,Xiao, Shangyue,Chu, Wenjing,Gao, Haiyan,Chu, Wenjing,Cao, Shifeng. 2017

[5]Headspace solid-phase microextraction-gas chromatography-mass spectrometry analysis of the volatile components of longan (Dimocarpus longan Lour.). Zhang, Yi,Gao, Bei,Zhang, Mingwei,Zhang, Yi,Gao, Bei,Zhang, Mingwei,Xu, Yujuan,Shi, John. 2009

[6]Allelopathic effects of allelochemicals of Ginkgo biloba leaf on fusarium wilt (Fusarium oxysporum) of hot pepper. Hou, Y. X.,Song, X. Y.,Yin, Y. L.,Li, Y. S.,Yang, J. S.,Zheng, J. Y.,Yin, Y. L.. 2016

[7]Characterization of Tectona grandis Extractives by GC-MS and IR and their Infusion into Rubberwood to Modify Dimensional Stability. Li, Jianing. 2017

[8]Chemical Composition and Antioxidant Activities of Three Polysaccharide Fractions from Pine Cones. Xu, Ren-Bo,Yang, Xin,Zhao, Hai-Tian,Lu, Wei-Hong,Cui, Jie,Cheng, Cui-Lin,Zou, Pan,Huang, Wei-Wei,Wang, Pu,Li, Wen-Jing,Hu, Xing-Long,Yang, Xin,Wang, Jing,Wang, Jing. 2012

[9]Simultaneous Determination of 69 Pesticide Residues in Coffee by Gas Chromatography-Mass Spectrometry. Yang, Xin,Xu, D. C.,Qiu, J. W.,Ma, Ying,Cui, J.,Yang, Xin,Wang, Jing. 2011

[10]Volatile flavor compounds, total polyphenolic contents and antioxidant activities of a China gingko wine. Wang, Xu,Xie, Kelin,Feng, Tao,Zhuang, Haining,Ye, Ran,Fang, Zhongxiang.

[11]Simultaneous determination of 118 pesticide residues in Chinese teas by gas chromatography-mass spectrometry. Yang, Xin,Xu, De Chang,Qiu, Jian Wei,Zhang, Hua,Zhang, Ying Chun,Dong, Ai Jun,Ma, Ying,Wang, Jing,Wang, Jing.

[12]Comparison of Compositions and Antimicrobial Activities of Essential Oils from Chemically Stimulated Agarwood, Wild Agarwood and Healthy Aquilaria sinensis (Lour.) Gilg Trees. Chen, Huaiqiong,Yang, Yun,Xue, Jian,Wei, Jianhe,Zhang, Zheng,Chen, Hongjiang,Chen, Huaiqiong,Yang, Yun,Xue, Jian,Wei, Jianhe,Zhang, Zheng,Chen, Hongjiang,Yang, Yun,Chen, Hongjiang,Yang, Yun,Chen, Hongjiang.

[13]A baseline study on lipid and fatty acid composition in the pearl oyster, Pinctada fucata. Shen, Ya-nan,Zhang, Bo,Jiang, Song,Liu, Bo-suo,Huang, Gui-ju,Yu, Da-hui,Shen, Ya-nan,Zhang, Bo,Jiang, Song,Liu, Bo-suo,Huang, Gui-ju,Yu, Da-hui,Shen, Ya-nan,Zhang, Bo,Jiang, Song,Liu, Bo-suo,Huang, Gui-ju,Yu, Da-hui,Shen, Ya-nan,Zhang, Dong-ling.

[14]GC-MS Analysis of Volatile Components in Chinese Wild Strawberry (F. nilgerrensis Schlecht.). Zhao, M. Z.,Wang, J.,Wang, Z. W.,Qian, Y. M.,Wu, W. M..

[15](+/-)-2-Hexanol from Pterocarpus indicus leaves as attractant for female Aleurodicus dispersus (Hemiptera: Aleyrodidae). Zheng, L. X.,Wu, W. J.,Fu, Y. G.. 2014

[16]Determination of Persistent Environmental Pollutants in Bee Pollen by Gas Chromatography-Mass Spectrometry Using a Modified QuEChERS Approach. Wei, Yue,Chen, Fang,Xue, Xiaofeng,Li, Yi,Jinhuizhou,Zhao, Liuwei,Cao, Weirui,Wu, Liming,Wei, Yue,Chen, Fang,Xue, Xiaofeng,Li, Yi,Jinhuizhou,Zhao, Liuwei,Cao, Weirui,Wu, Liming,Yu, Linsheng.

[17]Dissipation Rates and Final Residues of Kresoxim-Methyl in Strawberry and Soil. Jia, Chunhong,Zhu, Xiaodan,Zhao, Ercheng,He, Min,Yu, Pingzhong,Chen, Li. 2013

[18]Chinese leek (Allium tuberosum Rottler ex Sprengel) reduced disease symptom caused by root-knot nematode. Huang Yong-hong,Huang Yong-hong,Mao Zhen-chuan,Xie Bing-yan.

[19]Multiresidue method for determination of 88 pesticides in berry fruits using solid-phase extraction and gas chromatography-mass spectrometry: Determination of 88 pesticides in berries using SPE and GC-MS. Yang, X.,Zhang, H.,Zhang, Y. C.,Dong, A. J.,Zhao, H. T.,Cui, J.,Liu, Y.,Yang, X.,Wang, J.,Sun, C. H..

[20]Characterization and Determination of 2-(2-Phenylethyl)chromones in Agarwood by GC-MS. Mei, Wen-Li,Yang, De-Lan,Wang, Hao,Yang, Jin-Ling,Zeng, Yan-Bo,Guo, Zhi-Kai,Dong, Wen-Hua,Li, Wei,Dai, Hao-Fu,Mei, Wen-Li,Yang, De-Lan,Wang, Hao,Yang, Jin-Ling,Zeng, Yan-Bo,Guo, Zhi-Kai,Dong, Wen-Hua,Li, Wei,Dai, Hao-Fu.

作者其他论文 更多>>

微信小程序