Chitosan-poly(m-phenylenediamine)@Fe3O4 nanocomposite for magnetic solid-phase extraction of polychlorinated biphenyls from water samples

文献类型： 外文期刊

第一作者： Liao, Qie Gen

作者： Liao, Qie Gen;Wang, Dong Gen;Luo, Lin Guang

作者机构：

关键词： CS-PPD@Fe3O4 nanocomposite;Gas chromatography-triple quadrupole mass spectrometry;Magnetic solid-phase extraction;Polychlorinated biphenyl

期刊名称：ANALYTICAL AND BIOANALYTICAL CHEMISTRY （ 影响因子：4.142； 五年影响因子：3.863 ）

ISSN： 1618-2642

年卷期： 2014 年 406 卷 29 期

页码：

收录情况： SCI

摘要： A extraction medium based on chitosan-poly(m-phenylenediamine) (CS-PPD) @Fe3O4 nanocomposite was synthesized by chemical polymerization of m-phenylenediamine in the presence of chitosan coated magnetic nanocomposite, and for the first time, used as the sorbent for the magnetic solid-phase extraction (MSPE) of seven polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153, and PCB180) at trace levels in water samples. Gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS) was used for PCBs quantification and detection. Several factors related to MSPE efficiencies, such as type and amount of sorbent, extraction time, sample pH, and desorption conditions were investigated. Under the optimized conditions, an excellent linearity was observed in the range of 1.0-200 ng L-1 for PCB180, 0.5-200 ng L-1 for the other six PCBs with the correlation coefficients ranging from 0.9954 to 0.9993. The good recoveries at spiked levels of 10.0, 20.0, and 50.0 ng L-1 were obtained in the range of 94 %-108 %, and the coefficients of variations were less than 6 %. The proposed method was feasible, rapid, and easy to operate for the trace analysis of the PCBs in local aquaculture water, livestock breeding water, and sewage water samples.

分类号：

  • 相关文献

[1]Comparison of Enantioseparations of 19 Chiral Polychlorinated Biphenyls by 5 Different Polysaccharides Chiral Columns. Xu Na-Na,Mu Peng-Qian,Jia Qi,Chai Ting-Ting,Yin Zhi-Qiang,Shu-Ming, Yang,Jing, Qiu,Chai Ting-Ting. 2015

[2]Effect of long-term fertilization on humic redox mediators in multiple microbial redox reactions. Guo, Peng,Zhang, Chunfang,Zhang, Dongdong,Guo, Peng,Wang, Yi,Zhang, Dongdong,Yu, Xinwei,Zhang, Zhichao. 2018

[3]Recombinant protein, AlnA, combined with transgenic alfalfa remediates polychlorinated biphenyl-contaminated soils: efficiency and rhizosphere microbial community response. Su, Yu,Wang, Yan,Zhang, Junxing,Pan, Hongyu,Chen, Baoyu,Wang, Yan,Chen, Baoyu.

[4]The Determination of PAHs in Fish by GC-QqQ-MS/MS. Li, Hui-Dong,Wang, Wen-Bo,Chen, Zi-Lei,Ding Ruiyan,Fang Liping,Wang Fengen,Lu, Xiao,Huo, Lu-Ge,Yang, Guo-Sheng,Li, Hui-Dong,Wang, Wen-Bo,Chen, Zi-Lei,Ding Ruiyan,Fang Liping,Wang Fengen,Lu, Xiao,Li, Hui-Dong,Wang, Wen-Bo,Chen, Zi-Lei,Ding Ruiyan,Fang Liping,Wang Fengen,Lu, Xiao,Aboul-Enein, Hassan Y.. 2013

[5]Development of a SIDA-SPE-GC-MS/MS isotope dilution assay for the quantification of eugenol in water samples. Liu, Huan,Li, Jincheng,Wang, Chaoying,Liu, Huan,Li, Jincheng,Wang, Chaoying. 2018

[6]Ultrasound-assisted emulsification-microextraction for the sensitive determination of ethyl carbamate in alcoholic beverages. Liao, Qie Gen,Li, Wei Hong,Luo, Lin Guang. 2013

[7]Simultaneous determination of zearalenone and its derivatives in edible vegetable oil by gel permeation chromatography and gas chromatography-triple quadrupole mass spectrometry. Qian, Mingrong,Zhang, Hu,Wu, Liqin,Wang, Jianmei,Qian, Mingrong,Zhang, Hu,Wu, Liqin,Wang, Jianmei,Jin, Nuo,Jiang, Kezhi.

[8]Determination of twelve herbicides in tobacco by a combination of solid-liquid-solid dispersive extraction using multi-walled carbon nanotubes, dispersive liquid-liquid micro-extraction, and detection by GC with triple quadrupole mass spectrometry. Liao, Qie Gen,Zhou, Yao Min,Luo, Lin Guang,Wang, Li Bing,Feng, Xiao Hu.

[9]Magnetic metal-organic framework MIL-100(Fe) microspheres for the magnetic solid-phase extraction of trace polycyclic aromatic hydrocarbons from water samples. Du, Fuyou,Qin, Qun,Ruan, Guihua,Li, Jianping,Yang, Xianqing,Li, Laihao,Du, Fuyou,Ruan, Guihua,Li, Jianping.

[10]Multi-walled carbon nanotubes-based magnetic solid-phase extraction for the determination of zearalenone and its derivatives in maize by ultra-high performance liquid chromatography-tandem mass spectrometry. Han, Zheng,Fan, Zhichen,Dong, Maofeng,Guo, Wenbo,Fan, Kai,Zhao, Zhihui,Jiang, Keqiu,Wu, Yongjiang,Di Mavungu, Jose Diana,Campbell, Katrina.

[11]Determination of type A trichothecenes in coix seed by magnetic solid-phase extraction based on magnetic multi-walled carbon nanotubes coupled with ultra-high performance liquid chromatography-tandem mass spectrometry. Dong, Maofeng,Si, Wenshuai,Wang, Weimin,Bai, Bing,Nie, Dongxia,Song, Weiguo,Zhao, Zhihui,Han, Zheng,Guo, Yirong,Han, Zheng.

[12]Rapid Magnetic Solid-Phase Extraction Based on Monodisperse Magnetic Single-Crystal Ferrite Nanoparticles for the Determination of Free Fatty Acid Content in Edible Oils. Wei, Fang,Lv, Xin,Dong, Xu-Yan,Chen, Hong,Zhao, Qin,Feng, Yu-Qi.

[13]Rapid Magnetic Solid-Phase Extraction Based on Magnetic Multiwalled Carbon Nanotubes for the Determination of Polycyclic Aromatic Hydrocarbons in Edible Oils. Zhao, Qin,Luo, Yan-Bo,Ding, Jun,Xiao, Neng,Feng, Yu-Qi,Wei, Fang.

[14]One-pot synthesis of magnetic zeolitic imidazolate framework/grapheme oxide composites for the extraction of neonicotinoid insecticides from environmental water samples. Cao, Xiaolin,Jiang, Zejun,Wang, Shanshan,Hong, Sihui,Li, Hui,Shao, Yong,She, Yongxin,Wang, Jing,Jin, Fen,Jin, Maojun. 2017

[15]Magnetic solid-phase extraction based on graphene oxide for the determination of lignans in sesame oil. Wu, Linxia,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Dai, Xianhong,Chen, Xiaomei,Zhou, Haiyan,Bai, Yizhen,Ding, Jian,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Chen, Xiaomei,Zhou, Haiyan,Bai, Yizhen,Wu, Linxia,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Dai, Xianhong,Chen, Xiaomei,Ding, Jian,Wu, Linxia,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Dai, Xianhong,Chen, Xiaomei,Ding, Xiaoxia,Li, Peiwu,Zhou, Haiyan,Bai, Yizhen,Ding, Jian. 2017

[16]Rapid and Sensitive Detection of Avermectin Residues in Edible Oils by Magnetic Solid-Phase Extraction Combined with Ultra-High-Pressure Liquid Chromatography-Tandem Mass Spectrometry. Zhang, Hui-Xian,Xia, Hong,Gong, Yan,Peng, Xi-Tian,Lu, Wei,Peng, Xi-Tian,Feng, Yu-Qi.

[17]Determination of benzimidazole residues in animal tissue samples by combination of magnetic solid-phase extraction with capillary zone electrophoresis. Hu, Xi-Zhou,Chen, Ming-Luan,Gao, Qiang,Yu, Qiong-Wei,Feng, Yu-Qi,Hu, Xi-Zhou,Gao, Qiang.

作者其他论文 更多>>

微信小程序