Zeolite H-Beta as a Dispersive Solid-Phase Extraction Sorbent for the Determination of Eight Neonicotinoid Insecticides Using Ultra-High-Performance Liquid Chromatography-Tandem Mass Spectrometry
文献类型： 外文期刊
作者： Si, Wenshuai 1 ; Wang, Shouying 1 ; Bai, Bing 1 ; Wu, Nan 1 ; Ye, Tai 2 ; Xu, Fei 2 ; Kong, Cong 3 ;
作者机构： 1.Shanghai Acad Agr Sci, Inst Agrifood Stand & Testing Technol, 1000 Jinqi Rd, Shanghai 201403, Peoples R China
2.Univ Shanghai Sci & Technol, Sch Hlth Sci & Engn, 516 Jungong Rd, Shanghai 200093, Peoples R China
3.Chinese Acad Fishery Sci, East China Sea Fisheries Res Inst, Minist Agr & Rural Affairs, Key Lab East China Sea Fishery Resources Exploita, Shanghai 200090, Peoples R China
关键词： neonicotinoid; zeolite H-Beta; bottled water and honey products; liquid chromatography-tandem mass spectrometry; dispersive solid-phase extraction
期刊名称：APPLIED SCIENCES-BASEL （ 影响因子：2.838； 五年影响因子：2.921 ）
ISSN：
年卷期： 2022 年 12 卷 9 期
页码：
收录情况： SCI
摘要： In this study, a dispersive solid-phase extraction (DSPE) pretreatment procedure using zeolite H-Beta as a sorbent was exploited for the determination of eight neonicotinoids in bottled water and honey products based on ultra-high-performance liquid chromatography-tandem mass spectrometry analysis. The zeolite H-Beta was demonstrated to be a suitable sorbent for neonicotinoid insecticides, even after 10 recycles of reuse. The method performance was evaluated by the linearity (R-2 >= 0.998), recovery (71-108%), precision (0.1-7.8%), limit of detection (0.05-0.1 ng/mL) and limit of quantification (0.1-0.2 ng/mL), which suggested excellent stability and high sensitivity with the use of the DSPE procedure. The method was further successfully applied in the test of neonicotinoid insecticides in 34 samples. Zeolite H-Beta shows promise as an efficient and practical material for monitoring neonicotinoid insecticides in bottled water and multiplex honey matrices.
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