Multi-pharmaceuticals analysis in fish by continuous series solid-phase extraction coupled with UPLC-MS/MS
文献类型： 外文期刊
作者： Gao, Lei 1 ; Wang, Peng 1 ; Chen, Zhongxiang 1 ; Tang, Shizhan 1 ; Wu, Song 1 ; Li, Gang 3 ; Qin, Dongli 1 ;
作者机构： 1.Chinese Acad Fishery Sci, Heilongjiang River Fisheries Res Inst, 232 Hesong St, Harbin 150070, Peoples R China
2.Minist Agr & Rural Affairs, Key Lab Control Qual & Safety Aquat Prod, Beijing 100041, Peoples R China
3.Jilin Prov Fisheries Res Inst, 1195 Kunshan St, Changchun 130033, Peoples R China
关键词： series solid-phase extraction (s-SPE); ultra performance liquid chromatography triple quadruple tandem mass spectrometry (UPLC-MS/MS); multi-pharmaceuticals; fish; food safety
期刊名称：ACTA CHROMATOGRAPHICA （ 影响因子：2.011； 五年影响因子：1.35 ）
ISSN： 1233-2356
年卷期： 2022 年 34 卷 1 期
页码：
收录情况： SCI
摘要： Pharmaceuticals which are widely used in aquatic can easily migrate into the environment and aquatic animals, and can increase the risk of drug resistance and allergic symptoms if consumed by humans. In order to achieve high-throughput analysis of pharmaceuticals with different physical and chemical properties from complex matrices, we developed a new method for various types pharmaceuticals in fish and shrimp tissue. Series solid-phase extraction (s-SPE) with different adsorbents was selected for extracting and purifying analytes with different paddings. s-SPE were combined with ultra performance liquid chromatography triple quadruple tandem mass spectrometry (UPLC-MS/MS) for the detection of 30 pharmaceuticals antibiotics in fish samples. This method was stabilized and reliable to determinate the pharmaceuticals in fish and shrimp samples. As the method combined multiple Chinese national standards method, it could be easily treat the multi-pharmaceuticals from the fish and shrimp samples once time. It provided for both quantitative and qualitative methods and they could be applied to single- or multi-residue methods.
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