Rapid and sensitive analytical strategy for multi-class antibiotic residues analysis in aquatic products with amphiphilic magnetic polymer particles as an effective cleanup adsorbent
文献类型： 外文期刊
作者： Liu, Zhenzhen 1 ; Zhao, Huiyu 1 ; Wang, Jiao 1 ; Wang, Zhiwei 1 ; Di, Shanshan 1 ; Xu, Hao 1 ; Wang, Qiang 1 ; Wang, Xinhong 2 ; Wang, Xinquan 1 ; Qi, Peipei 1 ;
作者机构： 1.Zhejiang Acad Agr Sci, Inst Agroprod Safety & Nutr, State Key Lab Managing Biot & Chem Threats Qual &, Hangzhou 310021, Peoples R China
2.Xiamen Univ, Coll Environm & Ecol, State Key Lab Marine Environm Sci, Xiamen 361005, Peoples R China
3.Agr Minist Key Lab Pesticide Residue Detect, Hangzhou 310021, Peoples R China
4.Key Lab Detect Pesticide Residues & Control Zheji, Hangzhou 310021, Peoples R China
关键词： Magnetic particles; Multi -class antibiotic residues; Aquatic products; Liquid chromatography -tandem mass; spectrometry
期刊名称：FOOD CHEMISTRY （ 影响因子：8.8； 五年影响因子：8.6 ）
ISSN： 0308-8146
年卷期： 2023 年 400 卷
页码：
收录情况： SCI
摘要： Multi-class antibiotic analysis in aquatic products is still challenging owing to the complex matrix and low co -extraction efficiency of various antibiotics. A facile and sensitive sample pretreatment method based on mag-netic dispersive solid-phase extraction was thus developed via systematic optimization of extraction and puri-fication procedure. The multi-class antibiotics can simultaneously be extracted by acetonitrile-2 % acetic acid. Amphiphilic magnetic particles and C18 were used as adsorbents to remove matrix interferences, affording significantly reduced matrix effects of analytes. Under the optimum conditions, satisfactory linearity, recovery, precision, and sensitivity were achieved. The method limits of quantification were 0.25-0.5 mu g kg- 1. Besides, it displayed obvious advantages in operation convenience and efficiency due to the usage of magnetic particles. The developed method was successfully used to analyze antibiotic residues in both freshwater and seafood products, manifesting its suitability for antibiotic residues analysis in aquatic products.
- 相关文献
作者其他论文 更多>>
-
Insights into the adsorption performance and mechanism of novel 3D bimetallic MOF nanosheets for the high-efficient removal of 6PPD and 6PPD-quinone
作者：Wu, Nannan;Wang, Jiao;Liu, Zhenzhen;Zhao, Huiyu;Di, Shanshan;Wang, Zhiwei;Wang, Xinquan;Qi, Peipei;Zheng, Bing;Zheng, Bing;Di, Shanshan;Wang, Zhiwei;Wang, Xinquan;Qi, Peipei;Di, Shanshan;Wang, Zhiwei;Wang, Xinquan;Qi, Peipei
关键词：3D bimetallic MOFs; 6PPD; 6PPD-quinone; Adsorption mechanism; DFT calculations
-
Current-use pesticides monitoring and ecological risk assessment in vegetable soils at the provincial scale
作者：Zuo, Wei;Zhao, Yang;Qi, Peipei;Zhang, Chunrong;Zhao, Xueping;Wu, Shenggan;An, Xuehua;Liu, Xinju;Cheng, Xi;Tang, Tao;Yu, Yijun
关键词：Soil; Pesticide residue; Spatial distribution; Vegetable type; Ecological risk assessment
-
Long-term biogas slurry application increases microbial necromass but not plant lignin contribution to soil organic carbon in paddy soils as regulated by fungal community
作者：Chen, Zhaoming;Ma, Jinchuan;Ma, Junwei;Ye, Jing;Yu, Qiaogang;Zou, Ping;Sun, Wanchun;Lin, Hui;Wang, Feng;Wang, Qiang;Zhao, Xinlin
关键词：Soil organic carbon; Lignin phenols; Microbial necromass; Microbial community structure; Biogas slurry
-
Development and validation of modified QuEChERS method combined with LC-MS/MS for high-throughput analysis of per- and polyfluoroalkyl substances in fish samples
作者：Liu, Xiaoqi;Shi, Ranran;Liu, Juanjuan;Wang, Xinquan;Liu, Xiaoqi;Liu, Zhenzhen;Zhao, Huiyu;Shi, Ranran;Wang, Jiao;Liu, Juanjuan;Di, Shanshan;Wang, Zhiwei;Wang, Xinquan;Liu, Lianliang;Liu, Lianliang;Qi, Peipei
关键词：PFAS; Integrated QuEChERS; Liquid chromatography -tandem mass; spectrometry; Liquid chromatography-tandem mass; Fe3O4-TiO2
-
Enzymatic and transcriptional level changes induced by the co-presence of lead and procymidone in hook snout carp (Opsariichthys bidens)
作者：Wu, Shenggan;Di, Shanshan;Lv, Lu;Wang, Dou;Wang, Xinquan;Wang, Yanhua
关键词：Combined effect; Aquatic toxicology; Toxic mechanism; Gene expression
-
Review of fruits flavor deterioration in postharvest storage: Odorants, formation mechanism and quality control
作者：Zhao, Huiyu;Zhang, Suling;Ma, Di;Liu, Zhenzhen;Qi, Peipei;Wang, Zhiwei;Di, Shanshan;Wang, Xinquan;Wang, Xinquan
关键词：Fruit; Deterioration odorants; Influencing factors; Formation mechanism
-
Long-term successive biochar application increases plant lignin and microbial necromass accumulation but decreases their contributions to soil organic carbon in rice-wheat cropping system
作者：Chen, Zhaoming;He, Lili;Ma, Jinchuan;Ma, Junwei;Ye, Jing;Yu, Qiaogang;Zou, Ping;Sun, Wanchun;Lin, Hui;Wang, Feng;Wang, Qiang;Zhao, Xu
关键词：amino sugars; biochar; lignin phenols; microbial necromass; paddy field; soil organic carbon
