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Method validation and dissipation kinetics of the new HPPD inhibitor QYR301 in rice, paddy water and paddy soil using a QuEChERS-based method and LC-MS/MS

文献类型： 外文期刊

作者： Wane, Hengzhi 1 ; Sun, Penglei 1 ; Zhang, Xiaolin 1 ; Wang, Lipeng 1 ; Guo, Wenlei 3 ; Bei, Feng 4 ; Liu, Weitang 1 ; Wan 1 ;

作者机构： 1.Shandong Agr Univ, Coll Plant Protect, Tai An 271018, Shandong, Peoples R China

2.Shandong Agr Univ, Key Lab Pesticide Toxicol & Applicat Tech, Tai An 271018, Shandong, Peoples R China

3.Guangdong Acad Agr Sci, Plant Protect Res Inst, Guangdong Prov Key Lab High Technol Plant Protect, Guangzhou 510640, Guangdong, Peoples R China

4.Taian Customs, Tai An 271000, Shandong, Peoples R China

关键词： HPPD-Inhibiting herbicide; QYR301; Dissipation; Rice; LC-MS/MS; QuEChERS

期刊名称：ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY （ 影响因子：6.291； 五年影响因子：6.393 ）

ISSN： 0147-6513

年卷期： 2019 年 184 卷

页码：

收录情况： SCI

摘要： A rapid and simple method based on liquid chromatography-tandem mass spectrometry (LC-MS/MS) of sample preparation using QuEChERS was developed for detecting residues of QYR301, a new HPPD-inhibiting herbicide, in rice plant (straw), water, soil, rice hull and brown rice (BR). To eliminate matrix interference, matrix-matched calibrations with satisfactory linearity (R-2 > 0.99) were used for accurate quantification. The method showed recoveries of 90.3-108.1% and relative standard deviations (RSDs) < 11%. The limits of quantification (LOQ) for QYR301 were 0.005 mg kg(-1) in all five matrixes. Furthermore, the dissipation kinetics and terminal residues of QYR301 were determined at two sites in 2018. The days for 50% dissipation (DT50) of QYR301 in rice plants, water and soil were 3.6-4.4, 0.7-3.0 and 4.3-8.0 d, respectively, which indicated that QYR301 is a short-persistence herbicide. Moreover, no QYR301 residues were detected in BR, rice hull and straw collected at harvest following its application at 1.0 or 1.5 x of the recommended high rate. These results will help organizations and governments establish related principles/laws regarding the use of QYR301 in terms of environmental protection, food safety and other potential aspects.

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